Tetrachlorohydroquinone p-methoxybenzyl ether

Base Information

• Chemical Name: Tetrachlorohydroquinone p-methoxybenzyl ether
• CAS No.: 172796-92-8
• Molecular Formula: C₁₄H₁₀Cl₄O₃
• Molecular Weight: 368.044
• Mol file: 172796-92-8.mol

Synonyms:Tetrachlorohydroquinone p-methoxybenzyl ether

Chemical Property of Tetrachlorohydroquinone p-methoxybenzyl ether

Chemical Property:

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Technology Process of Tetrachlorohydroquinone p-methoxybenzyl ether

There total 6 articles about Tetrachlorohydroquinone p-methoxybenzyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

trimethyl(4-methoxybenzyloxy)silane (14629-56-2) + chloranil (118-75-2) → Tetrachlorohydroquinone p-methoxybenzyl ether (172796-92-8)

Guidance literature:

In acetonitrile; at 40 ℃; for 3h; Irradiation;

DOI:10.1021/jo00129a044

Reference yield: 25.0%

trimethyl(4-methoxybenzyloxy)silane (14629-56-2) + chloranil (118-75-2) → Tetrachlorohydroquinone bis(trimethylsilyl) ether (17258-75-2) + Tetrachlorohydroquinone mono(trimethylsilyl) ether + Tetrachlorohydroquinone p-methoxybenzyl ether (172796-92-8) + Trimethyl-[2,3,5,6-tetrachloro-4-(4-methoxy-benzyloxy)-phenoxy]-silane

Guidance literature:

In dichloromethane; at 40 ℃; for 3h; Yield given. Title compound not separated from byproducts; Irradiation;

DOI:10.1021/jo00129a044

Reference yield: 6.0%

trimethyl(4-methoxybenzyloxy)silane (14629-56-2) + chloranil (118-75-2) → Tetrachlorohydroquinone p-methoxybenzyl ether (172796-92-8) + Trimethyl-[2,3,5,6-tetrachloro-4-(4-methoxy-benzyloxy)-phenoxy]-silane + 2,3,5,6-Tetrachloro-4-[(4-methoxy-phenyl)-trimethylsilanyl-methoxy]-phenol (172796-88-2) + 1,2,4,5-Tetrachloro-3-[(4-methoxy-phenyl)-trimethylsilanyl-methoxy]-6-trimethylsilanyloxy-benzene

Guidance literature:

In dichloromethane; at 40 ℃; for 3h; Further byproducts given; Irradiation;

DOI:10.1021/jo00129a044

upstream raw materials:

trimethyl(4-methoxybenzyloxy)silane

chloranil

2,3,5,6-tetrachlorobenzene-1,4-diol

4-methoxybenzylmagnesium chloride