4(1H)-Pyrimidinone, 5,6-dihydroxy-2-methyl- (9CI)

Base Information

• Chemical Name: 4(1H)-Pyrimidinone, 5,6-dihydroxy-2-methyl- (9CI)
• CAS No.: 98021-25-1
• Molecular Formula: C₅H₆N₂O₃
• Molecular Weight: 142.114
• Mol file: 98021-25-1.mol

Synonyms:4(1H)-Pyrimidinone,5,6-dihydroxy-2-methyl- (9CI); 4,5,6-Pyrimidinetriol, 2-methyl- (6CI)

Chemical Property of 4(1H)-Pyrimidinone, 5,6-dihydroxy-2-methyl- (9CI)

Chemical Property:

• PSA: 86.21000
• LogP: -0.51050

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4(1H)-Pyrimidinone, 5,6-dihydroxy-2-methyl- (9CI)

There total 4 articles about 4(1H)-Pyrimidinone, 5,6-dihydroxy-2-methyl- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methyl-4,6-dihydroxypyrimidine (1194-22-5) → 5-hydroxy-2-methyl-(3H)-pyrimidin-4-one (24614-14-0) + 5,6-dihydroxy-2-methyl-(3H)-pyrimidin-4-one (98021-25-1) + 5,6-dihydro-5,6-dihydroxy-2-methyl-(3H)-pyrimidin-4-one + bis(5-hydro-5,6-dihydroxy-2-methyl-(3H)-pyrimidin-4-one-6-yl)

Guidance literature:

With hydroxyl radical; pH=4.5; Kinetics;

DOI:10.1021/jp0117720

Reference yield:

2-methyl-5-tetrahydropyran-2-yloxy-1H-pyrimidine-4,6-dione → 5,6-dihydroxy-2-methyl-(3H)-pyrimidin-4-one (98021-25-1)

Guidance literature:

With acetic acid;

DOI:10.1039/jr9560002124

Reference yield:

5-benzyloxy-2-methyl-1H-pyrimidine-4,6-dione → 5,6-dihydroxy-2-methyl-(3H)-pyrimidin-4-one (98021-25-1)

Guidance literature:

With palladium; acetic acid; Hydrogenation;

upstream raw materials:

2-methyl-4,6-dihydroxypyrimidine

acetamide hydrochloride

2-hydroxy-malonic acid diethyl ester

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