methyl 2,3-diethanethio-5-[4'-(p-fluorophenyl)-1'H-1',2',3'-triazol-1'-yl]-2,3,5-trideoxy-β-D-ribofuranoside

Base Information

Chemical Name:methyl 2,3-diethanethio-5-[4'-(p-fluorophenyl)-1'H-1',2',3'-triazol-1'-yl]-2,3,5-trideoxy-β-D-ribofuranoside
CAS No.:1234261-82-5
Molecular Formula:C₁₈H₂₄FN₃O₂S₂
Molecular Weight:397.538
Hs Code.:

Synonyms:methyl 2,3-diethanethio-5-[4'-(p-fluorophenyl)-1'H-1',2',3'-triazol-1'-yl]-2,3,5-trideoxy-β-D-ribofuranoside

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Chemical Property of methyl 2,3-diethanethio-5-[4'-(p-fluorophenyl)-1'H-1',2',3'-triazol-1'-yl]-2,3,5-trideoxy-β-D-ribofuranoside

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Technology Process of methyl 2,3-diethanethio-5-[4'-(p-fluorophenyl)-1'H-1',2',3'-triazol-1'-yl]-2,3,5-trideoxy-β-D-ribofuranoside

There total 1 articles about methyl 2,3-diethanethio-5-[4'-(p-fluorophenyl)-1'H-1',2',3'-triazol-1'-yl]-2,3,5-trideoxy-β-D-ribofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 766-98-3
1-ethynyl-4-fluorobenzene

: 1234261-80-3
methyl 5-azido-2,3,5-trideoxy-2,3-diethanethio-β-D-ribofuranoside

: 1234261-82-5
methyl 2,3-diethanethio-5-[4'-(p-fluorophenyl)-1'H-1',2',3'-triazol-1'-yl]-2,3,5-trideoxy-β-D-ribofuranoside

Guidance literature:: With copper; copper(II) sulfate; In water; tert-butyl alcohol; at 20 ℃;
DOI:10.1016/j.ejmech.2010.03.038

Reference yield: 83.0%

: 1234261-82-5
methyl 2,3-diethanethio-5-[4'-(p-fluorophenyl)-1'H-1',2',3'-triazol-1'-yl]-2,3,5-trideoxy-β-D-ribofuranoside

: 7288-28-0
2,4-bis(trimethylsiloxy)-5-methylpyrimidine

: 1234262-00-0
1-[2',3'-diethanethio-5'-[4''-(p-fluorophenyl)-1''H-1'',2'',3''-triazol-1''-yl]-2',3',5'-trideoxy-β-D-ribofuranosyl]thymine

Guidance literature:: methyl 2,3-diethanethio-5-[4'-(p-fluorophenyl)-1'H-1',2',3'-triazol-1'-yl]-2,3,5-trideoxy-β-D-ribofuranoside; 2,4-bis(trimethylsiloxy)-5-methylpyrimidine; With trimethylsilyl trifluoromethanesulfonate; In acetonitrile; at 0 - 20 ℃; for 12.5h;

With water; sodium hydrogencarbonate; In dichloromethane; acetonitrile;
DOI:10.1016/j.ejmech.2010.03.038

Reference yield: 82.0%

: 1234261-82-5
methyl 2,3-diethanethio-5-[4'-(p-fluorophenyl)-1'H-1',2',3'-triazol-1'-yl]-2,3,5-trideoxy-β-D-ribofuranoside

: 10457-14-4
O,O'-bis-(trimethylsilyl)uracil

: 1234261-91-6
1-[2',3'-diethanethio-5'-[4''-(p-fluorophenyl)-1''H-1'',2'',3''-triazol-1''-yl]-2',3',5'-trideoxy-β-D-ribofuranosyl]uracil

Guidance literature:: methyl 2,3-diethanethio-5-[4'-(p-fluorophenyl)-1'H-1',2',3'-triazol-1'-yl]-2,3,5-trideoxy-β-D-ribofuranoside; O,O'-bis-(trimethylsilyl)uracil; With trimethylsilyl trifluoromethanesulfonate; In acetonitrile; at 0 - 20 ℃; for 12.5h;

With water; sodium hydrogencarbonate; In dichloromethane; acetonitrile;
DOI:10.1016/j.ejmech.2010.03.038