2,4(1H,3H)-Pyrimidinedione,5-fluorodihydro-6-hydroxy-,cis-(9CI)

Base Information

• Chemical Name: 2,4(1H,3H)-Pyrimidinedione,5-fluorodihydro-6-hydroxy-,cis-(9CI)
• CAS No.: 93713-26-9
• Molecular Formula: C4H5 F N2 O3
• Molecular Weight: 148.094
• Hs Code.: 2933599090
• Mol file: 93713-26-9.mol

Synonyms:2,4(1H,3H)-Pyrimidinedione,5-fluorodihydro-6-hydroxy-,cis-(9CI)

Chemical Property of 2,4(1H,3H)-Pyrimidinedione,5-fluorodihydro-6-hydroxy-,cis-(9CI)

Chemical Property:

• PSA: 78.43000
• Density: 1.63±0.1 g/cm3 (20 °C, 760 mmHg)
• LogP: -0.86010

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,4(1H,3H)-Pyrimidinedione,5-fluorodihydro-6-hydroxy-,cis-(9CI)

There total 3 articles about 2,4(1H,3H)-Pyrimidinedione,5-fluorodihydro-6-hydroxy-,cis-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

uracil (66-22-8,144104-68-7,18324-22-6,27072-01-1,2920-92-5,51953-19-6) → 5-fluorouracil (51-21-8) + (+/-)-cis-5-Fluor-6-hydroxy-5,6-dihydrouracil (37103-91-6,93713-25-8,93713-26-9) + (5S,6S)-5-Fluoro-6-hydroxy-dihydro-pyrimidine-2,4-dione (37103-91-6,93713-25-8,93713-26-9) + cis-5-fluoro-6-acetoxy-5,6-dihydrouracil (56311-36-5,100814-55-9,100814-58-2)

Guidance literature:

With acetyl hypofluorite; In water-d2; Yield given. Further byproducts given. Yields of byproduct given;

Reference yield: 10.0%

uracil (66-22-8,144104-68-7,18324-22-6,27072-01-1,2920-92-5,51953-19-6) → 5-fluorouracil (51-21-8) + (+/-)-cis-5-Fluor-6-hydroxy-5,6-dihydrouracil (37103-91-6,93713-25-8,93713-26-9) + (5S,6S)-5-Fluoro-6-hydroxy-dihydro-pyrimidine-2,4-dione (37103-91-6,93713-25-8,93713-26-9) + cis-5-fluoro-6-acetoxy-5,6-dihydrouracil (56311-36-5,100814-55-9,100814-58-2)

Guidance literature:

With acetyl hypofluorite; In water-d2; Yield given. Further byproducts given. Yields of byproduct given;

Reference yield:

acetic acid (64-19-7,77671-22-8) + uracil (66-22-8,144104-68-7,18324-22-6,27072-01-1,2920-92-5,51953-19-6) → 5-fluorouracil (51-21-8) + 5,5-difluoro-6-acetoxy-5,6-dihydrouracil (100814-61-7) + (5S,6R)-5-Fluoro-6-hydroxy-dihydro-pyrimidine-2,4-dione (93713-26-9) + Acetic acid (4S,5S)-5-fluoro-2,6-dioxo-hexahydro-pyrimidin-4-yl ester (100814-58-2) + Acetic acid (4R,5S)-5-fluoro-2,6-dioxo-hexahydro-pyrimidin-4-yl ester (100814-55-9) + 5-fluoro-6-hydroxy-dihydro-pyrimidine-2,4-dione (93713-25-8)

Guidance literature:

With fluorine; Product distribution; Mechanism; other reagents;

DOI:10.1021/jo00359a015

upstream raw materials:

uracil

acetic acid

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