(2-methoxynaphthalen-1-yl)(phenyl)sulfane

Base Information

• Chemical Name: (2-methoxynaphthalen-1-yl)(phenyl)sulfane
• CAS No.: 108979-03-9
• Molecular Formula: C₁₇H₁₄OS
• Molecular Weight: 266.364
• Mol file: 108979-03-9.mol

Synonyms:(2-methoxynaphthalen-1-yl)(phenyl)sulfane

Chemical Property of (2-methoxynaphthalen-1-yl)(phenyl)sulfane

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of (2-methoxynaphthalen-1-yl)(phenyl)sulfane

There total 13 articles about (2-methoxynaphthalen-1-yl)(phenyl)sulfane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

2-Methoxynaphthalene (93-04-9) + sodium phenylsulfonate (515-42-4) → (2-methoxynaphthalen-1-yl)(phenyl)sulfane (108979-03-9)

Guidance literature:

With hydrogenchloride; In water; at 80 ℃; for 6h;

Reference yield: 97.0%

2-Methoxynaphthalene (93-04-9) + sodium benzenesulfonate (873-55-2) → (2-methoxynaphthalen-1-yl)(phenyl)sulfane (108979-03-9)

Guidance literature:

With hydrogenchloride; 1-hexyl-3-methyl-1-imidazolium bromide; In water; at 80 ℃; for 6h; chemoselective reaction;

DOI:10.1039/c6ob02823c

Reference yield: 90.0%

racemic methyl phenyl sulfoxide (1193-82-4) + β-naphthol (135-19-3) → (2-methoxynaphthalen-1-yl)(phenyl)sulfane (108979-03-9)

Guidance literature:

racemic methyl phenyl sulfoxide; β-naphthol; With trifluoromethylsulfonic anhydride; In acetonitrile; at 0 ℃; for 3h; Green chemistry;

With potassium phosphate; In water; at 70 ℃; for 24h; Micellar solution; Green chemistry;

DOI:10.1039/c6sc04504a

upstream raw materials:

1-bromo-2-methoxynaphthalene

sodium thiophenolate

2-methoxynaphthylamine

thiophenol

Downstream raw materials:

1-benzenesulfonyl-2-methoxy-naphthalene