methyl 2-(3-chloro-4-(4-(2,4-dichlorophenylsulfonamido)-1-(2,4-dichlorophenylsulfonyl)-2-methyl-1H-benzo[d]imidazol-5-yloxy)phenyl)acetate

Base Information

Chemical Name:methyl 2-(3-chloro-4-(4-(2,4-dichlorophenylsulfonamido)-1-(2,4-dichlorophenylsulfonyl)-2-methyl-1H-benzo[d]imidazol-5-yloxy)phenyl)acetate
CAS No.:1080522-38-8
Molecular Formula:C₂₉H₂₀Cl₅N₃O₇S₂
Molecular Weight:763.891
Hs Code.:

Synonyms:methyl 2-(3-chloro-4-(4-(2,4-dichlorophenylsulfonamido)-1-(2,4-dichlorophenylsulfonyl)-2-methyl-1H-benzo[d]imidazol-5-yloxy)phenyl)acetate

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Chemical Property of methyl 2-(3-chloro-4-(4-(2,4-dichlorophenylsulfonamido)-1-(2,4-dichlorophenylsulfonyl)-2-methyl-1H-benzo[d]imidazol-5-yloxy)phenyl)acetate

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Technology Process of methyl 2-(3-chloro-4-(4-(2,4-dichlorophenylsulfonamido)-1-(2,4-dichlorophenylsulfonyl)-2-methyl-1H-benzo[d]imidazol-5-yloxy)phenyl)acetate

There total 6 articles about methyl 2-(3-chloro-4-(4-(2,4-dichlorophenylsulfonamido)-1-(2,4-dichlorophenylsulfonyl)-2-methyl-1H-benzo[d]imidazol-5-yloxy)phenyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1080522-36-6
methyl 2-(4-(4-amino-2-methyl-1H-benzo[d]imidazol-5-yloxy)-3-chlorophenyl)acetate

: 16271-33-3
2,4-Dichlorobenzenesulfonyl chloride

: 1080522-38-8
methyl 2-(3-chloro-4-(4-(2,4-dichlorophenylsulfonamido)-1-(2,4-dichlorophenylsulfonyl)-2-methyl-1H-benzo[d]imidazol-5-yloxy)phenyl)acetate

Guidance literature:: With pyridine; at 20 ℃; for 3h;

Reference yield:

: 118469-15-1
5-fluoro-2-methyl-1H-benzo[d]imidazole

: 1080522-38-8
methyl 2-(3-chloro-4-(4-(2,4-dichlorophenylsulfonamido)-1-(2,4-dichlorophenylsulfonyl)-2-methyl-1H-benzo[d]imidazol-5-yloxy)phenyl)acetate

Guidance literature:: Multi-step reaction with 5 steps

1.1: sulfuric acid; nitric acid / 1 h / 0 °C

1.2: 0 °C

2.1: potassium fluoride on basic alumina / 18-crown-6 ether / dimethyl sulfoxide / 20 h / 80 °C

2.2: pH 5

3.1: sulfuric acid / 2.5 h / Heating / reflux

4.1: water; tin(ll) chloride / ethyl acetate / 16 h / 20 °C

5.1: pyridine / 3 h / 20 °C

With pyridine; sulfuric acid; potassium fluoride on basic alumina; water; nitric acid; tin(ll) chloride; 18-crown-6 ether; sulfuric acid; In dimethyl sulfoxide; ethyl acetate;

Reference yield:

: 1080522-30-0
5-fluoro-2-methyl-4-nitro-1H-benzo[d]imidazole

: 1080522-38-8
methyl 2-(3-chloro-4-(4-(2,4-dichlorophenylsulfonamido)-1-(2,4-dichlorophenylsulfonyl)-2-methyl-1H-benzo[d]imidazol-5-yloxy)phenyl)acetate

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium fluoride on basic alumina / 18-crown-6 ether / dimethyl sulfoxide / 20 h / 80 °C

1.2: pH 5

2.1: sulfuric acid / 2.5 h / Heating / reflux

3.1: water; tin(ll) chloride / ethyl acetate / 16 h / 20 °C

4.1: pyridine / 3 h / 20 °C

With pyridine; potassium fluoride on basic alumina; water; tin(ll) chloride; 18-crown-6 ether; sulfuric acid; In dimethyl sulfoxide; ethyl acetate;