1-(3-bromo-2,3-dideoxy-2-fluoro-5-O-trityl-β-D-arabinofuranosyl)-5-ethyluracil

Base Information

Chemical Name:1-(3-bromo-2,3-dideoxy-2-fluoro-5-O-trityl-β-D-arabinofuranosyl)-5-ethyluracil
CAS No.:1383568-01-1
Molecular Formula:C₃₀H₂₈BrFN₂O₄
Molecular Weight:579.466
Hs Code.:

Synonyms:1-(3-bromo-2,3-dideoxy-2-fluoro-5-O-trityl-β-D-arabinofuranosyl)-5-ethyluracil

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Chemical Property of 1-(3-bromo-2,3-dideoxy-2-fluoro-5-O-trityl-β-D-arabinofuranosyl)-5-ethyluracil

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Technology Process of 1-(3-bromo-2,3-dideoxy-2-fluoro-5-O-trityl-β-D-arabinofuranosyl)-5-ethyluracil

There total 4 articles about 1-(3-bromo-2,3-dideoxy-2-fluoro-5-O-trityl-β-D-arabinofuranosyl)-5-ethyluracil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 1251064-60-4
1-(2-deoxy-2-fluoro-3-O-mesyl-5-O-trityl-β-D-arabinofuranosyl)-5-ethyluracil

: 1383568-01-1
1-(3-bromo-2,3-dideoxy-2-fluoro-5-O-trityl-β-D-arabinofuranosyl)-5-ethyluracil

Guidance literature:: With sodium bromide; In N,N-dimethyl-formamide; at 110 ℃; for 24h;
DOI:10.1016/j.bmc.2012.05.004

Reference yield:

: 1006598-55-5
1-(2-deoxy-2-fluoro-5-O-trityl-β-D-arabinofuranosyl)-5-ethyluracil

: 1383568-01-1
1-(3-bromo-2,3-dideoxy-2-fluoro-5-O-trityl-β-D-arabinofuranosyl)-5-ethyluracil

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 48 h / Cooling

2: sodium bromide / N,N-dimethyl-formamide / 24 h / 110 °C

With pyridine; sodium bromide; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2012.05.004

Reference yield:

: 76-83-5
trityl chloride

: 1383568-01-1
1-(3-bromo-2,3-dideoxy-2-fluoro-5-O-trityl-β-D-arabinofuranosyl)-5-ethyluracil

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; dmap / 8 h / 80 °C

2: pyridine / 48 h / Cooling

3: sodium bromide / N,N-dimethyl-formamide / 24 h / 110 °C

With pyridine; dmap; sodium bromide; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2012.05.004