1-(2-deoxy-2-fluoro-3-O-mesyl-5-O-trityl-β-D-arabinofuranosyl)-5-ethyluracil

Base Information

Chemical Name:1-(2-deoxy-2-fluoro-3-O-mesyl-5-O-trityl-β-D-arabinofuranosyl)-5-ethyluracil
CAS No.:1251064-60-4
Molecular Formula:C₃₁H₃₁FN₂O₇S
Molecular Weight:594.661
Hs Code.:

Synonyms:1-(2-deoxy-2-fluoro-3-O-mesyl-5-O-trityl-β-D-arabinofuranosyl)-5-ethyluracil

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Chemical Property of 1-(2-deoxy-2-fluoro-3-O-mesyl-5-O-trityl-β-D-arabinofuranosyl)-5-ethyluracil

Chemical Property:

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Technology Process of 1-(2-deoxy-2-fluoro-3-O-mesyl-5-O-trityl-β-D-arabinofuranosyl)-5-ethyluracil

There total 3 articles about 1-(2-deoxy-2-fluoro-3-O-mesyl-5-O-trityl-β-D-arabinofuranosyl)-5-ethyluracil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1006598-55-5
1-(2-deoxy-2-fluoro-5-O-trityl-β-D-arabinofuranosyl)-5-ethyluracil

: 124-63-0
methanesulfonyl chloride

: 1251064-60-4
1-(2-deoxy-2-fluoro-3-O-mesyl-5-O-trityl-β-D-arabinofuranosyl)-5-ethyluracil

Guidance literature:: With pyridine; at 0 ℃;
DOI:10.1021/jm100803c

Reference yield:

: 76-83-5
trityl chloride

: 1251064-60-4
1-(2-deoxy-2-fluoro-3-O-mesyl-5-O-trityl-β-D-arabinofuranosyl)-5-ethyluracil

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; dmap / 8 h / 80 °C

2: pyridine / 48 h / Cooling

With pyridine; dmap;
DOI:10.1016/j.bmc.2012.05.004

Reference yield:

: 83546-42-3
FEAU

: 1251064-60-4
1-(2-deoxy-2-fluoro-3-O-mesyl-5-O-trityl-β-D-arabinofuranosyl)-5-ethyluracil

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; dmap / 8 h / 80 °C

2: pyridine / 48 h / Cooling

With pyridine; dmap;
DOI:10.1016/j.bmc.2012.05.004