(R)-(+)-2-((Phenylthio)methyl)-2-(3,4-dimethoxyphenyl)cyclobutanone ethylene acetal

Base Information

Chemical Name:(R)-(+)-2-((Phenylthio)methyl)-2-(3,4-dimethoxyphenyl)cyclobutanone ethylene acetal
CAS No.:158531-91-0
Molecular Formula:C₂₁H₂₄O₄S
Molecular Weight:372.485
Hs Code.:

Synonyms:(R)-(+)-2-((Phenylthio)methyl)-2-(3,4-dimethoxyphenyl)cyclobutanone ethylene acetal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-(+)-2-((Phenylthio)methyl)-2-(3,4-dimethoxyphenyl)cyclobutanone ethylene acetal

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Technology Process of (R)-(+)-2-((Phenylthio)methyl)-2-(3,4-dimethoxyphenyl)cyclobutanone ethylene acetal

There total 8 articles about (R)-(+)-2-((Phenylthio)methyl)-2-(3,4-dimethoxyphenyl)cyclobutanone ethylene acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 107-21-1
ethylene glycol

: 158531-90-9
(R)-(+)-2-((Phenylthio)methyl)-2-(3,4-dimethoxyphenyl)cyclobutanone

: 158531-91-0
(R)-(+)-2-((Phenylthio)methyl)-2-(3,4-dimethoxyphenyl)cyclobutanone ethylene acetal

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 4.5h; Heating;
DOI:10.1016/S0040-4039(00)78256-6

Reference yield:

: 107-21-1
ethylene glycol

: 2-((Phenylthio)methyl)-2-(3,4-dimethoxyphenyl)cyclobutanone

: 158531-91-0
(R)-(+)-2-((Phenylthio)methyl)-2-(3,4-dimethoxyphenyl)cyclobutanone ethylene acetal

: (S)-(-)-2-((Phenylthio)methyl)-2-(3,4-dimethoxyphenyl)cyclobutanone ethylene acetal

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 4.5h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Heating;
DOI:10.1021/jo00126a030

Reference yield:

: 107-21-1
ethylene glycol

: 2-(4,5-Dimethoxy-2-(trimethylsilyl)phenyl)-2-((phenylthio)methyl)cyclobutanone

: 158531-91-0
(R)-(+)-2-((Phenylthio)methyl)-2-(3,4-dimethoxyphenyl)cyclobutanone ethylene acetal

: (S)-(-)-2-((Phenylthio)methyl)-2-(3,4-dimethoxyphenyl)cyclobutanone ethylene acetal

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 4.5h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Heating;
DOI:10.1021/jo00126a030