2-pentadecyl-(3-O-benzyl-4-O-chloroacetyl-1,2-dideoxy-6-O-palmitoyl-α-D-glucopyrano)-<2,1-d>-2-oxazoline

Base Information

Chemical Name:2-pentadecyl-(3-O-benzyl-4-O-chloroacetyl-1,2-dideoxy-6-O-palmitoyl-α-D-glucopyrano)-<2,1-d>-2-oxazoline
CAS No.:78835-46-8
Molecular Formula:C₄₇H₇₈ClNO₇
Molecular Weight:804.592
Hs Code.:

Synonyms:2-pentadecyl-(3-O-benzyl-4-O-chloroacetyl-1,2-dideoxy-6-O-palmitoyl-α-D-glucopyrano)-<2,1-d>-2-oxazoline

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Chemical Property of 2-pentadecyl-(3-O-benzyl-4-O-chloroacetyl-1,2-dideoxy-6-O-palmitoyl-α-D-glucopyrano)-<2,1-d>-2-oxazoline

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Technology Process of 2-pentadecyl-(3-O-benzyl-4-O-chloroacetyl-1,2-dideoxy-6-O-palmitoyl-α-D-glucopyrano)-<2,1-d>-2-oxazoline

There total 8 articles about 2-pentadecyl-(3-O-benzyl-4-O-chloroacetyl-1,2-dideoxy-6-O-palmitoyl-α-D-glucopyrano)-<2,1-d>-2-oxazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 78835-46-8
2-pentadecyl-(3-O-benzyl-4-O-chloroacetyl-1,2-dideoxy-6-O-palmitoyl-α-D-glucopyrano)-<2,1-d>-2-oxazoline

Guidance literature:: Multi-step reaction with 6 steps

1: 94 percent / barium oxide, barium hydroxide / dimethylformamide

2: 80 percent / 80 percent aq. acetic acid / Heating

3: 88 percent / pyridine / 2 h / from -15 deg C to RT

4: tris(triphenylphosphine)rhodium(I) chloride

5: 84 percent / pyridine; CH₂Cl₂ / 0.17 h / 0 °C

6: mercuric chloride, mercuric oxide / acetonitrile

With pyridine; barium dihydroxide; acetic acid; mercury dichloride; mercury(II) oxide; barium(II) oxide; Wilkinson's catalyst; In pyridine; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0008-6215(00)80408-5

Reference yield:

: 78835-37-7
allyl 2-deoxy-2-(palmitoylamino)-β-D-glucopyranoside

: 78835-46-8
2-pentadecyl-(3-O-benzyl-4-O-chloroacetyl-1,2-dideoxy-6-O-palmitoyl-α-D-glucopyrano)-<2,1-d>-2-oxazoline

Guidance literature:: Multi-step reaction with 7 steps

1: 85 percent / zinc chloride

2: 94 percent / barium oxide, barium hydroxide / dimethylformamide

3: 80 percent / 80 percent aq. acetic acid / Heating

4: 88 percent / pyridine / 2 h / from -15 deg C to RT

5: tris(triphenylphosphine)rhodium(I) chloride

6: 84 percent / pyridine; CH₂Cl₂ / 0.17 h / 0 °C

7: mercuric chloride, mercuric oxide / acetonitrile

With pyridine; barium dihydroxide; acetic acid; mercury dichloride; mercury(II) oxide; zinc(II) chloride; barium(II) oxide; Wilkinson's catalyst; In pyridine; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0008-6215(00)80408-5

Reference yield:

: 78835-43-5
allyl 3-O-benzyl-6-O-palmitoyl-2-deoxy-2-(palmitoylamino)-β-D-glucopyranoside

: 78835-46-8
2-pentadecyl-(3-O-benzyl-4-O-chloroacetyl-1,2-dideoxy-6-O-palmitoyl-α-D-glucopyrano)-<2,1-d>-2-oxazoline

Guidance literature:: Multi-step reaction with 3 steps

1: tris(triphenylphosphine)rhodium(I) chloride

2: 84 percent / pyridine; CH₂Cl₂ / 0.17 h / 0 °C

3: mercuric chloride, mercuric oxide / acetonitrile

With mercury dichloride; mercury(II) oxide; Wilkinson's catalyst; In pyridine; dichloromethane; acetonitrile;
DOI:10.1016/S0008-6215(00)80408-5