Technology Process of 4-benzyloxy-2,6-bis(4,4-dimethyl-4,5-dihydrooxazol-2-yl)pyridine
There total 1 articles about 4-benzyloxy-2,6-bis(4,4-dimethyl-4,5-dihydrooxazol-2-yl)pyridine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
benzyl alcohol;
With
sodium hydride;
In
tetrahydrofuran;
at 20 ℃;
for 0.166667h;
Inert atmosphere;
C15H18ClN3O2;
In
tetrahydrofuran;
at 20 ℃;
for 0.5h;
Inert atmosphere;
DOI:10.1016/j.tetlet.2009.09.021
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: palladium 10% on activated carbon; hydrogen / methanol / 4 h / 20 °C
2.1: potassium hydroxide / N,N-dimethyl-formamide / 0.17 h / 20 °C / Inert atmosphere
2.2: 2 h / 20 °C / Inert atmosphere
3.1: potassium carbonate / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere
With
palladium 10% on activated carbon; hydrogen; potassium carbonate; potassium hydroxide;
In
methanol; N,N-dimethyl-formamide;
DOI:10.1039/c0ob00887g
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: palladium 10% on activated carbon; hydrogen / methanol / 4 h / 20 °C
2.1: potassium hydroxide / N,N-dimethyl-formamide / 0.17 h / 20 °C / Inert atmosphere
2.2: 2 h / 20 °C / Inert atmosphere
3.1: potassium carbonate / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere
4.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere
With
palladium 10% on activated carbon; hydrogen; potassium carbonate; potassium hydroxide;
In
methanol; N,N-dimethyl-formamide;
DOI:10.1039/c0ob00887g
