tert-butyl N-<5-<(E)-3-(4-methoxyphenyl)prop-2-enoyl>-8-<<(E)-4-(4-methoxyphenyl)prop-2-enoyl>amino>-5-<(1,4-13C2)azaoctyl>>carbamate

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Chemical Name:tert-butyl N-<5-<(E)-3-(4-methoxyphenyl)prop-2-enoyl>-8-<<(E)-4-(4-methoxyphenyl)prop-2-enoyl>amino>-5-<(1,4-13C2)azaoctyl>>carbamate
CAS No.:219985-79-2
Molecular Formula:C₃₂H₄₃N₃O₆
Molecular Weight:567.688
Hs Code.:

Synonyms:tert-butyl N-<5-<(E)-3-(4-methoxyphenyl)prop-2-enoyl>-8-<<(E)-4-(4-methoxyphenyl)prop-2-enoyl>amino>-5-<(1,4-13C2)azaoctyl>>carbamate

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Chemical Property of tert-butyl N-<5-<(E)-3-(4-methoxyphenyl)prop-2-enoyl>-8-<<(E)-4-(4-methoxyphenyl)prop-2-enoyl>amino>-5-<(1,4-13C2)azaoctyl>>carbamate

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Technology Process of tert-butyl N-<5-<(E)-3-(4-methoxyphenyl)prop-2-enoyl>-8-<<(E)-4-(4-methoxyphenyl)prop-2-enoyl>amino>-5-<(1,4-13C2)azaoctyl>>carbamate

There total 5 articles about tert-butyl N-<5-<(E)-3-(4-methoxyphenyl)prop-2-enoyl>-8-<<(E)-4-(4-methoxyphenyl)prop-2-enoyl>amino>-5-<(1,4-13C2)azaoctyl>>carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 34446-64-5,42996-84-9
(E)-3-(4-methoxyphenyl)propenoyl chloride

: 219985-78-1
-(1,4-13C2)butyl>>carbamate

: 219985-79-2
tert-butyl N-<5-<(E)-3-(4-methoxyphenyl)prop-2-enoyl>-8-<<(E)-4-(4-methoxyphenyl)prop-2-enoyl>amino>-5-<(1,4-13C2)azaoctyl>>carbamate

Guidance literature:: With triethylamine; In ethyl acetate; at 25 ℃;
DOI:10.1016/S0040-4020(98)01014-X

Reference yield:

: 943-89-5
(E)-3-(4-methoxyphenyl)acrylic acid

: 219985-79-2
tert-butyl N-<5-<(E)-3-(4-methoxyphenyl)prop-2-enoyl>-8-<<(E)-4-(4-methoxyphenyl)prop-2-enoyl>amino>-5-<(1,4-13C2)azaoctyl>>carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / oxalyl chloride / toluene

2: 54 percent / Et₃N / ethyl acetate / 25 °C

With oxalyl dichloride; triethylamine; In ethyl acetate; toluene;
DOI:10.1016/S0040-4020(98)01014-X

Reference yield:

: 219985-72-5
(1-13C)propyl>carbamate

: 219985-79-2
tert-butyl N-<5-<(E)-3-(4-methoxyphenyl)prop-2-enoyl>-8-<<(E)-4-(4-methoxyphenyl)prop-2-enoyl>amino>-5-<(1,4-13C2)azaoctyl>>carbamate

Guidance literature:: Multi-step reaction with 4 steps

1: NaOH, Raney-Ni, H₂ / ethanol; H₂O / 20 h / 25 °C / 2068.59 Torr

2: 91 percent / methanol / 25 °C

3: NaOH, Raney-Ni, H₂ / aq. ethanol / 20 h / 25 °C / 2068.59 Torr

4: 54 percent / Et₃N / ethyl acetate / 25 °C

With sodium hydroxide; hydrogen; nickel; triethylamine; In methanol; ethanol; water; ethyl acetate;
DOI:10.1016/S0040-4020(98)01014-X