chlorure de l'acide N-acetoxy chloro-2 phenyl-2 acetohydroximique

Base Information

• Chemical Name: chlorure de l'acide N-acetoxy chloro-2 phenyl-2 acetohydroximique
• CAS No.: 14113-33-8
• Molecular Formula: C₁₀H₉Cl₂NO₂
• Molecular Weight: 246.093
• Mol file: 14113-33-8.mol

Synonyms:chlorure de l'acide N-acetoxy chloro-2 phenyl-2 acetohydroximique

Chemical Property of chlorure de l'acide N-acetoxy chloro-2 phenyl-2 acetohydroximique

Chemical Property:

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Technology Process of chlorure de l'acide N-acetoxy chloro-2 phenyl-2 acetohydroximique

There total 12 articles about chlorure de l'acide N-acetoxy chloro-2 phenyl-2 acetohydroximique which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

(2-nitroethenyl)benzene (102-96-5) + acetyl chloride (75-36-5) → chlorure de l'acide N-acetoxy chloro-2 phenyl-2 acetohydroximique (14113-33-8)

Guidance literature:

With titanium tetrachloride; In dichloromethane; at 0 ℃; for 5h; Product distribution; other Lewis acid;

Reference yield: 85.0%

acetic anhydride (108-24-7) + chlorure de l'acide chloro-2 phenyl-2 acetohidroximique (77130-73-5) → chlorure de l'acide N-acetoxy chloro-2 phenyl-2 acetohydroximique (14113-33-8)

Guidance literature:

at 100 ℃; for 2h;

DOI:10.1016/0040-4020(80)80224-9

Reference yield: 75.0%

(2-nitroethenyl)benzene (102-96-5) + acetyl chloride (75-36-5) → rac-3-chloroindolin-2-one (68235-96-1) + chlorure de l'acide N-acetoxy chloro-2 phenyl-2 acetohydroximique (14113-33-8)

Guidance literature:

With iron(III) chloride; In dichloromethane; at 0 ℃; for 5h;

upstream raw materials:

(2-nitroethenyl)benzene

acetic anhydride

chlorure de l'acide chloro-2 phenyl-2 acetohidroximique

acetyl chloride