Odcissviiqqcdn-uhfffaoysa-

Base Information

Chemical Name:Odcissviiqqcdn-uhfffaoysa-
CAS No.:244237-05-6
Molecular Formula:C₁₅H₈BrNO₃
Molecular Weight:330.137
Hs Code.:
DSSTox Substance ID:DTXSID801252650
Nikkaji Number:J1.130.250E

Synonyms:ODCISSVIIQQCDN-UHFFFAOYSA-;DTXSID801252650;244237-05-6;6-Bromo-4-hydroxy-2-phenyl-5,8-quinolinedione;InChI=1/C15H8BrNO3/c16-9-6-12(19)14-13(15(9)20)11(18)7-10(17-14)8-4-2-1-3-5-8/h1-7H,(H,17,18)

Suppliers and Price of Odcissviiqqcdn-uhfffaoysa-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of Odcissviiqqcdn-uhfffaoysa-

Chemical Property:

XLogP3:2.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:1
Exact Mass:328.96876
Heavy Atom Count:20
Complexity:607

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)C2=CC(=O)C3=C(N2)C(=O)C=C(C3=O)Br

Technology Process of Odcissviiqqcdn-uhfffaoysa-

There total 3 articles about Odcissviiqqcdn-uhfffaoysa- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 244237-01-2
6-bromo-4-hydroxy-5,8-dimethoxy-2-phenylquinoline

: 244237-05-6
6-bromo-4-hydroxy-2-phenylquinoline-5,8-dione

Guidance literature:: With ammonium cerium(IV) nitrate; In water; acetonitrile; at 0 ℃; for 0.5h;
DOI:10.3987/com-99-8549

Reference yield:

: 94-02-0
ethyl 3-oxo-3-phenylpropionate

: 244237-05-6
6-bromo-4-hydroxy-2-phenylquinoline-5,8-dione

Guidance literature:: Multi-step reaction with 4 steps

2: 93 percent / pyridinium p-toluenesulfonate / CHCl₃ / 18 h / Heating

3: 89 percent / xylene / 11 h / 300 °C / sealed tube

4: 52 percent / cerium ammonium nitrate / acetonitrile; H₂O / 0.5 h / 0 °C

With ammonium cerium(IV) nitrate; pyridinium p-toluenesulfonate; In chloroform; water; acetonitrile; xylene; 1: amination / 2: Substitution / 3: Cyclization / 4: Oxidation;
DOI:10.3987/com-99-8549

Reference yield:

: ethyl 3-(4-bromo-2,5-dimethoxyphenylamino)-3-phenyl-2-propenoate

: 244237-05-6
6-bromo-4-hydroxy-2-phenylquinoline-5,8-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / xylene / 11 h / 300 °C / sealed tube

2: 52 percent / cerium ammonium nitrate / acetonitrile; H₂O / 0.5 h / 0 °C

With ammonium cerium(IV) nitrate; In water; acetonitrile; xylene; 1: Cyclization / 2: Oxidation;
DOI:10.3987/com-99-8549