N-<6-(2,3-dimethoxyphenyl)-2-(dimethylamino)-3-cyclohexen-1-yl>benzamide

Base Information

• Chemical Name: N-<6-(2,3-dimethoxyphenyl)-2-(dimethylamino)-3-cyclohexen-1-yl>benzamide
• CAS No.: 141944-39-0
• Molecular Formula: C₂₃H₂₈N₂O₃
• Molecular Weight: 380.487

Synonyms:N-<6-(2,3-dimethoxyphenyl)-2-(dimethylamino)-3-cyclohexen-1-yl>benzamide

Chemical Property of N-<6-(2,3-dimethoxyphenyl)-2-(dimethylamino)-3-cyclohexen-1-yl>benzamide

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Technology Process of N-<6-(2,3-dimethoxyphenyl)-2-(dimethylamino)-3-cyclohexen-1-yl>benzamide

There total 5 articles about N-<6-(2,3-dimethoxyphenyl)-2-(dimethylamino)-3-cyclohexen-1-yl>benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

benzoyl chloride (98-88-4) + 6-(2,3-dimethoxyphenyl)-N2,N2-dimethyl-3-cyclohexene-1,2-diamine (141944-32-3) → N-<6-(2,3-dimethoxyphenyl)-2-(dimethylamino)-3-cyclohexen-1-yl>benzamide (141944-39-0)

Guidance literature:

With sodium hydroxide; In chloroform; at 10 - 15 ℃; for 0.75h;

DOI:10.1002/jhet.5570290106

Reference yield:

N,N-dimethyl-1,3-butadien-1-amine (139943-10-5,1515-77-1) → N-<6-(2,3-dimethoxyphenyl)-2-(dimethylamino)-3-cyclohexen-1-yl>benzamide (141944-39-0)

Guidance literature:

Multi-step reaction with 3 steps

1: 66 percent / hydroquinone / CHCl₃ / 20 h / Ambient temperature

2: glacial acetic acid, Zn / 20 h / Ambient temperature

3: 78 percent / 10percent aq. NaOH / CHCl₃ / 0.75 h / 10 - 15 °C

With sodium hydroxide; acetic acid; hydroquinone; zinc; In chloroform;

DOI:10.1002/jhet.5570290106

Reference yield:

2,3-dimethoxynitrostyrene (2815-67-0) → N-<6-(2,3-dimethoxyphenyl)-2-(dimethylamino)-3-cyclohexen-1-yl>benzamide (141944-39-0)

Guidance literature:

Multi-step reaction with 3 steps

1: 66 percent / hydroquinone / CHCl₃ / 20 h / Ambient temperature

2: glacial acetic acid, Zn / 20 h / Ambient temperature

3: 78 percent / 10percent aq. NaOH / CHCl₃ / 0.75 h / 10 - 15 °C

With sodium hydroxide; acetic acid; hydroquinone; zinc; In chloroform;

DOI:10.1002/jhet.5570290106

upstream raw materials:

benzoyl chloride

6-(2,3-dimethoxyphenyl)-N²,N²-dimethyl-3-cyclohexene-1,2-diamine

N,N-dimethyl-1,3-butadien-1-amine

2,3-dimethoxynitrostyrene

Downstream raw materials:

1,4,4a,10b-tetrahydro-9,10-dimethoxy-N,N-dimethyl-6-phenyl-4-phenanthridinamine hydrochloride

1,4,4a,5,6,10b-hexahydro-9,10-dimethoxy-N,N-dimethyl-6-phenyl-4-phenanthridinamine

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