N¹,N³,N⁵-Trimethyl-N¹,N³,N⁵-tris(3-nitrophenyl)benzene-1,3,5-tricarboxamide

Base Information

• Chemical Name: N¹,N³,N⁵-Trimethyl-N¹,N³,N⁵-tris(3-nitrophenyl)benzene-1,3,5-tricarboxamide
• CAS No.: 940301-03-1
• Molecular Formula: C₃₀H₂₄N₆O₉
• Molecular Weight: 612.555
• Mol file: 940301-03-1.mol

Synonyms:N¹,N³,N⁵-Trimethyl-N¹,N³,N⁵-tris(3-nitrophenyl)benzene-1,3,5-tricarboxamide

Chemical Property of N¹,N³,N⁵-Trimethyl-N¹,N³,N⁵-tris(3-nitrophenyl)benzene-1,3,5-tricarboxamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N¹,N³,N⁵-Trimethyl-N¹,N³,N⁵-tris(3-nitrophenyl)benzene-1,3,5-tricarboxamide

There total 2 articles about N¹,N³,N⁵-Trimethyl-N¹,N³,N⁵-tris(3-nitrophenyl)benzene-1,3,5-tricarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

methyl iodide (74-88-4) → N1,N3,N5-Trimethyl-N1,N3,N5-tris(3-nitrophenyl)benzene-1,3,5-tricarboxamide (940301-03-1)

Guidance literature:

benzene-1,3,5-tricarboxylic acid tris[(3-nitrophenyl)amide]; With lithium hexamethyldisilazane; In tetrahydrofuran; for 0.5h;

methyl iodide; In tetrahydrofuran; at 20 ℃; for 18h;

Reference yield: 95.0%

N-methyl-3-nitroaniline (619-26-1) + 1,3,5-benzene tris(carbonyl chloride) (4422-95-1) → N1,N3,N5-Trimethyl-N1,N3,N5-tris(3-nitrophenyl)benzene-1,3,5-tricarboxamide (940301-03-1)

Guidance literature:

In acetonitrile; at 90 ℃; for 48h;

DOI:10.1016/j.chempr.2019.06.023

Reference yield: 83.0%

N1,N3,N5-Trimethyl-N1,N3,N5-tris(3-nitrophenyl)benzene-1,3,5-tricarboxamide (940301-03-1) → N1,N3,N5-tris(3-aminophenyl)-N1,N3,N5-trimethylbenzene-1,3,5-tricarboxamide (940301-04-2)

Guidance literature:

With palladium 10% on activated carbon; hydrazine hydrate; In ethanol; at 95 ℃; Microwave irradiation;

DOI:10.1016/j.chempr.2019.06.023

upstream raw materials:

methyl iodide

N-methyl-3-nitroaniline

1,3,5-benzene tris(carbonyl chloride)

Downstream raw materials:

N¹,N³,N⁵-tris(3-aminophenyl)-N¹,N³,N⁵-trimethylbenzene-1,3,5-tricarboxamide