(-)-5,6-O-CYCLOHEXYLIDENE-D-ISOASCORBIC ACID

Base Information

Chemical Name:(-)-5,6-O-CYCLOHEXYLIDENE-D-ISOASCORBIC ACID
CAS No.:97627-84-4
Molecular Formula:C12H16 O6
Molecular Weight:256.25184
Hs Code.:2932999099
Mol file:97627-84-4.mol

Synonyms:1,4-Dioxaspiro[4.5]decane,D-erythro-hex-2-enonic acid deriv.; 5,6-O-Cyclohexylidene-D-erythorbic acid;5,6-O-Cyclohexylidene-D-isoascorbic acid

Suppliers and Price of (-)-5,6-O-CYCLOHEXYLIDENE-D-ISOASCORBIC ACID

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
(-)-5,6-O-CYCLOHEXYLIDENE-D-ISOASCORBIC ACID 95.00%
5MG
$ 499.33

Total 1 raw suppliers

Chemical Property of (-)-5,6-O-CYCLOHEXYLIDENE-D-ISOASCORBIC ACID

Chemical Property:

Melting Point:177-179 °C
PSA：85.22000
LogP:1.31520

Purity/Quality:

99% ^*data from raw suppliers

(-)-5,6-O-CYCLOHEXYLIDENE-D-ISOASCORBIC ACID 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:
Safety Statements: 22-24/25

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (-)-5,6-O-CYCLOHEXYLIDENE-D-ISOASCORBIC ACID

There total 3 articles about (-)-5,6-O-CYCLOHEXYLIDENE-D-ISOASCORBIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 933-40-4
cycloxexanone dimethyl ketal

: 89-65-6,98966-42-8
isoascorbic acid

: 97627-84-4
5,6-O-Cyclohexylidene-D-isoascorbic acid

Guidance literature:: With tin(ll) chloride; In ethyl acetate; for 0.5h; Heating;
DOI:10.1016/S0957-4166(00)82119-9

Reference yield: 88.0%

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 26094-91-7,98966-42-8
L-arabo-ascorbic acid

: 6614-52-4,97627-84-4
5,6-O-cycloheyxlidene-(L)-ascorbic acid

Guidance literature:: With boron trifluoride diethyl etherate; orthoformic acid triethyl ester; Ambient temperature;

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 89-65-6,98966-42-8
isoascorbic acid

: 97627-84-4
5,6-O-Cyclohexylidene-D-isoascorbic acid

Guidance literature:: With toluene-4-sulfonic acid; orthoformic acid triethyl ester; Yield given. Multistep reaction; 1.) ethyl acetate, reflux, 30 min; 2.) reflux, 5 h;
DOI:10.1055/s-1987-28008