3-4)-tri-O-benzyl-β-D-glucopyranosyl>prop-1-ene

Base Information

• Chemical Name: 3-4)-tri-O-benzyl-β-D-glucopyranosyl>prop-1-ene
• CAS No.: 193553-11-6
• Molecular Formula: C₆₄H₆₈O₁₀
• Molecular Weight: 997.238

Synonyms:3-4)-tri-O-benzyl-β-D-glucopyranosyl>prop-1-ene

Chemical Property of 3-4)-tri-O-benzyl-β-D-glucopyranosyl>prop-1-ene

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Technology Process of 3-4)-tri-O-benzyl-β-D-glucopyranosyl>prop-1-ene

There total 6 articles about 3-4)-tri-O-benzyl-β-D-glucopyranosyl>prop-1-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

benzyl bromide (100-39-0) + 3-4)-O-β-D-glucopyranosyl>prop-1-ene (222420-62-4) → 3-4)-tri-O-benzyl-β-D-glucopyranosyl>prop-1-ene (193553-11-6)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; for 12h; Ambient temperature;

DOI:10.1016/S0040-4020(98)01177-6

Reference yield: 64.0%

(2S,3R,4S,5R,6R)-2-Allyloxy-3,4-bis-benzyloxy-6-benzyloxymethyl-5-((2S,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-ol → 3-4)-tri-O-benzyl-β-D-glucopyranosyl>prop-1-ene (193553-11-6)

Guidance literature:

With triethylsilane; boron trifluoride diethyl etherate; In acetonitrile; at -30 ℃; for 0.5h;

DOI:10.1071/C97015

Reference yield: 56.3%

benzyl bromide (100-39-0) + allyl O-β-D-glucopyranosyl-(1->4)-β-D-glucopyranoside (52211-61-7,113842-87-8,114495-87-3,93752-82-0) → 3-4)-tri-O-benzyl-β-D-glucopyranosyl>prop-1-ene (193553-11-6)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; paraffin;

upstream raw materials:

benzyl bromide

allyl O-β-D-glucopyranosyl-(1->4)-β-D-glucopyranoside

3-4)-O-β-D-glucopyranosyl>prop-1-ene

2,3,6-tri-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-D-glucono-1,5-lactone

Downstream raw materials:

2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl-(1→4)-2,3,6-tri-O-benzyl-α-D-glucopyranose

C₆₁H₆₃BrO₁₀

1-O-(4-O-β-D-glucopyranosyl-α-D-glucopyranosyl)-3-deoxy-2(R)-glycerol

1-O-(4-O-β-D-glucopyranosyl-α-D-glucopyranosyl)-3-deoxy-2(S)-glycerol

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