α-acetoxy-1-(allyloxycarbonyl)-2-benzyl-2-(3-butenyl)hydrazineacetic acid methyl ester

Base Information

Chemical Name:α-acetoxy-1-(allyloxycarbonyl)-2-benzyl-2-(3-butenyl)hydrazineacetic acid methyl ester
CAS No.:155219-95-7
Molecular Formula:C₂₀H₂₆N₂O₆
Molecular Weight:390.436
Hs Code.:

Synonyms:α-acetoxy-1-(allyloxycarbonyl)-2-benzyl-2-(3-butenyl)hydrazineacetic acid methyl ester

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Chemical Property of α-acetoxy-1-(allyloxycarbonyl)-2-benzyl-2-(3-butenyl)hydrazineacetic acid methyl ester

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Technology Process of α-acetoxy-1-(allyloxycarbonyl)-2-benzyl-2-(3-butenyl)hydrazineacetic acid methyl ester

There total 5 articles about α-acetoxy-1-(allyloxycarbonyl)-2-benzyl-2-(3-butenyl)hydrazineacetic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-52-7
benzaldehyde

: 155219-95-7
α-acetoxy-1-(allyloxycarbonyl)-2-benzyl-2-(3-butenyl)hydrazineacetic acid methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 94 percent / toluene / 18 h / Ambient temperature

2: 99 percent / pTSA, NaBH₃CN / tetrahydrofuran / 3.5 h / Ambient temperature

3: 39 percent / K₂CO₃, LiI / ethanol / 18 h / Heating

4: toluene / 5 h

5: pyridine / DMAP / 18 h / Ambient temperature

With pyridine; sodium cyanoborohydride; potassium carbonate; toluene-4-sulfonic acid; lithium iodide; dmap; In tetrahydrofuran; ethanol; toluene;
DOI:10.1016/S0040-4020(01)96267-2

Reference yield:

: N'-[1-Phenyl-meth-(E)-ylidene]-hydrazinecarboxylic acid allyl ester

: 155219-95-7
α-acetoxy-1-(allyloxycarbonyl)-2-benzyl-2-(3-butenyl)hydrazineacetic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / pTSA, NaBH₃CN / tetrahydrofuran / 3.5 h / Ambient temperature

2: 39 percent / K₂CO₃, LiI / ethanol / 18 h / Heating

3: toluene / 5 h

4: pyridine / DMAP / 18 h / Ambient temperature

With pyridine; sodium cyanoborohydride; potassium carbonate; toluene-4-sulfonic acid; lithium iodide; dmap; In tetrahydrofuran; ethanol; toluene;
DOI:10.1016/S0040-4020(01)96267-2

Reference yield:

: 155219-78-6
1-benzyl-2-hydrazinecarboxylic acid allyl ester

: 155219-95-7
α-acetoxy-1-(allyloxycarbonyl)-2-benzyl-2-(3-butenyl)hydrazineacetic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 39 percent / K₂CO₃, LiI / ethanol / 18 h / Heating

2: toluene / 5 h

3: pyridine / DMAP / 18 h / Ambient temperature

With pyridine; potassium carbonate; lithium iodide; dmap; In ethanol; toluene;
DOI:10.1016/S0040-4020(01)96267-2