3-phenyl-5-(((2,2,6,6-tetramethylpiperidin-1-yl)oxy)methyl)-4,5-dihydroisoxazole

Base Information

Chemical Name:3-phenyl-5-(((2,2,6,6-tetramethylpiperidin-1-yl)oxy)methyl)-4,5-dihydroisoxazole
CAS No.:1403477-92-8
Molecular Formula:C₁₉H₂₈N₂O₂
Molecular Weight:316.444
Hs Code.:

Synonyms:3-phenyl-5-(((2,2,6,6-tetramethylpiperidin-1-yl)oxy)methyl)-4,5-dihydroisoxazole

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Chemical Property of 3-phenyl-5-(((2,2,6,6-tetramethylpiperidin-1-yl)oxy)methyl)-4,5-dihydroisoxazole

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Technology Process of 3-phenyl-5-(((2,2,6,6-tetramethylpiperidin-1-yl)oxy)methyl)-4,5-dihydroisoxazole

There total 10 articles about 3-phenyl-5-(((2,2,6,6-tetramethylpiperidin-1-yl)oxy)methyl)-4,5-dihydroisoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 2564-83-2,45842-10-2,126517-51-9,25657-03-8,26933-82-4,54637-06-8,64104-42-3
2,2,6,6-Tetramethyl-1-piperidinyloxy free radical

: 68843-67-4
(E)-1-phenylbut-3-en-1-one oxime

: 1403477-92-8
3-phenyl-5-(((2,2,6,6-tetramethylpiperidin-1-yl)oxy)methyl)-4,5-dihydroisoxazole

Guidance literature:: With [hydroxy(tosyloxy)iodo]benzene; iron(II) diacetylacetonate; In dichloromethane; at 20 ℃; for 6h;
DOI:10.1039/c9ob02424g

Reference yield: 90.0%

: 68843-67-4
1-phenyl-but-3-en-1-one oxime

: 2564-83-2,45842-10-2,126517-51-9,25657-03-8,26933-82-4,54637-06-8,64104-42-3
2,2,6,6-Tetramethyl-1-piperidinyloxy free radical

: 1403477-92-8
3-phenyl-5-(((2,2,6,6-tetramethylpiperidin-1-yl)oxy)methyl)-4,5-dihydroisoxazole

Guidance literature:: With diethylazodicarboxylate; In toluene; at 50 ℃; for 20h; Inert atmosphere;
DOI:10.1002/anie.201203799

Reference yield: 83.0%

: 68843-67-4
1-phenyl-but-3-en-1-one oxime

: 887144-94-7
Togni's reagent II

: 2564-83-2
2,2,6,6-tetramethyl-piperidine-N-oxyl

: 1403477-92-8
3-phenyl-5-(((2,2,6,6-tetramethylpiperidin-1-yl)oxy)methyl)-4,5-dihydroisoxazole

Guidance literature:: With sodium acetate; copper(l) chloride; In N,N-dimethyl-formamide; at 50 ℃; for 0.5h; Inert atmosphere;
DOI:10.1039/c3cc42588f