(η3-cyclooctenyl)tris(methoxydiphenylphosphine)ruthenium(II) hexafluorophosphate

Base Information

Chemical Name:(η3-cyclooctenyl)tris(methoxydiphenylphosphine)ruthenium(II) hexafluorophosphate
CAS No.:82641-02-9
Molecular Formula:C₄₇H₅₂O₃P₃Ru*F₆P
Molecular Weight:1003.88
Hs Code.:

Synonyms:(η3-cyclooctenyl)tris(methoxydiphenylphosphine)ruthenium(II) hexafluorophosphate

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Chemical Property of (η3-cyclooctenyl)tris(methoxydiphenylphosphine)ruthenium(II) hexafluorophosphate

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Technology Process of (η3-cyclooctenyl)tris(methoxydiphenylphosphine)ruthenium(II) hexafluorophosphate

There total 2 articles about (η3-cyclooctenyl)tris(methoxydiphenylphosphine)ruthenium(II) hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 61003-57-4
hydrido(cycloocta-1,5-diene)tris(methoxydiphenylphosphine)ruthenium(II) hexafluoroborate

: 82641-02-9
(η3-cyclooctenyl)tris(methoxydiphenylphosphine)ruthenium(II) hexafluorophosphate

Guidance literature:: In ethanol; Heating methanol suspn. of complex for ca. 10 min at 50°C;;

Reference yield: 80.0%

: 4020-99-9
diphenylphosphinous acid methyl ester

: 61042-65-7
(cyclo-octa-1,5-diene)tris(N',N'-dimethylhydrazine)hydridorutheniumhexafluorophosphate

: 82641-02-9
(η3-cyclooctenyl)tris(methoxydiphenylphosphine)ruthenium(II) hexafluorophosphate

Guidance literature:: In methanol; Phosphine was added to a soln. of complex in dry, degassed MeOH at 25°C (N2 atm.);;

Reference yield: 71.0%

: 82641-02-9
Ru(C₈H₁₃)(P(OCH₃)(C₆H₅)2)3⁽¹⁺⁾*PF₆^(1-)=(Ru(C₈H₁₃)(P(OCH₃)(C₆H₅)2)3)PF₆

: 876938-53-3
Cyclohepta-1,3-diene

: 100562-79-6
Ru(C₇H₁₁)(P(OCH₃)(C₆H₅)2)3⁽¹⁺⁾*PF₆^(1-)=(Ru(C₇H₁₁)(P(OCH₃)(C₆H₅)2)3)PF₆

Guidance literature:: In methanol; 1,3-cycloheptadiene was added under N2 to a suspn. of Ru-complex in MeOH, mixt. was refluxed for ca. 2 h; ppt. was collected, recrystd. from CH2Cl2-EtOH; elem. anal.;
DOI:10.1016/0022-328X(85)88010-4