5-methyl-5-(4'-nitrophenyl)dipyrromethane

Base Information

• Chemical Name: 5-methyl-5-(4'-nitrophenyl)dipyrromethane
• CAS No.: 951032-07-8
• Molecular Formula: C₁₆H₁₅N₃O₂
• Molecular Weight: 281.314
• Mol file: 951032-07-8.mol

Synonyms:5-methyl-5-(4'-nitrophenyl)dipyrromethane

Chemical Property of 5-methyl-5-(4'-nitrophenyl)dipyrromethane

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 5-methyl-5-(4'-nitrophenyl)dipyrromethane

There total 1 articles about 5-methyl-5-(4'-nitrophenyl)dipyrromethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

pyrrole (109-97-7,30604-81-0) + (4-nitrophenyl)ethanone (100-19-6) → 5-methyl-5-(4'-nitrophenyl)dipyrromethane (951032-07-8)

Guidance literature:

With L-Tartaric acid; N,N'-Dimethylurea; In neat (no solvent); at 70 ℃; Green chemistry;

DOI:10.1039/d1gc01515j

Reference yield: 89.0%

5-methyl-5-(4'-nitrophenyl)dipyrromethane (951032-07-8) → C16H17N3 (1379805-23-8)

Guidance literature:

With palladium 10% on activated carbon; hydrazine hydrate; In ethanol; for 1h; Reflux;

DOI:10.1021/ja307791j

Reference yield: 33.0%

5-methyl-5-(4'-nitrophenyl)dipyrromethane (951032-07-8) + pyrrole (109-97-7,30604-81-0) + acetone (67-64-1) → C33H37N5O2 (1422191-89-6)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1021/ja307791j

upstream raw materials:

pyrrole

(4-nitrophenyl)ethanone

Downstream raw materials:

C₃₅H₄₅Cl₂N₅OPtS

C₃₅H₄₅Cl₂N₅OPtS

C₁₆H₁₇N₃

C₃₃H₃₉N₅