methyl 2-azido-3-O-benzyl-2-deoxy-4-O-methyl-6-O-trityl-α-D-glucopyranoside

Base Information

Chemical Name:methyl 2-azido-3-O-benzyl-2-deoxy-4-O-methyl-6-O-trityl-α-D-glucopyranoside
CAS No.:1428556-01-7
Molecular Formula:C₃₄H₃₅N₃O₅
Molecular Weight:565.669
Hs Code.:

Synonyms:methyl 2-azido-3-O-benzyl-2-deoxy-4-O-methyl-6-O-trityl-α-D-glucopyranoside

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Chemical Property of methyl 2-azido-3-O-benzyl-2-deoxy-4-O-methyl-6-O-trityl-α-D-glucopyranoside

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Technology Process of methyl 2-azido-3-O-benzyl-2-deoxy-4-O-methyl-6-O-trityl-α-D-glucopyranoside

There total 5 articles about methyl 2-azido-3-O-benzyl-2-deoxy-4-O-methyl-6-O-trityl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1428556-00-6
methyl 2-azido-3-O-benzyl-2-deoxy-6-O-trityl-α-D-glucopyranoside

: 74-88-4
methyl iodide

: 1428556-01-7
methyl 2-azido-3-O-benzyl-2-deoxy-4-O-methyl-6-O-trityl-α-D-glucopyranoside

Guidance literature:: methyl 2-azido-3-O-benzyl-2-deoxy-6-O-trityl-α-D-glucopyranoside; With sodium hydroxide; In dimethyl sulfoxide; at 20 ℃; for 0.25h; Inert atmosphere;

methyl iodide; In dimethyl sulfoxide; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1080/07328303.2012.722738

Reference yield:

: methyl 3-O-benzyl-4,6-O-benzylidene-α-D-mannopyranoside

: 1428556-01-7
methyl 2-azido-3-O-benzyl-2-deoxy-4-O-methyl-6-O-trityl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1.1: pyridine / dichloromethane / -15 °C

2.1: sodium azide / N,N-dimethyl-formamide / 20 °C

3.1: acetic acid / 2 h / 100 °C

4.1: pyridine / 20 °C

5.1: sodium hydroxide / dimethyl sulfoxide / 0.25 h / 20 °C / Inert atmosphere

5.2: 0.5 h / 20 °C / Inert atmosphere

With pyridine; sodium azide; acetic acid; sodium hydroxide; In dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1080/07328303.2012.722738

Reference yield:

: methyl 2-azido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside

: 1428556-01-7
methyl 2-azido-3-O-benzyl-2-deoxy-4-O-methyl-6-O-trityl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid / 2 h / 100 °C

2.1: pyridine / 20 °C

3.1: sodium hydroxide / dimethyl sulfoxide / 0.25 h / 20 °C / Inert atmosphere

3.2: 0.5 h / 20 °C / Inert atmosphere

With pyridine; acetic acid; sodium hydroxide; In dimethyl sulfoxide;
DOI:10.1080/07328303.2012.722738