N-fluorenylmethyloxycarbonyl-O-(2,3-di-O-benzoyl-β-D-xylopyranosyl)-L-serine benzyl ester

Base Information

• Chemical Name: N-fluorenylmethyloxycarbonyl-O-(2,3-di-O-benzoyl-β-D-xylopyranosyl)-L-serine benzyl ester
• CAS No.: 1415218-13-1
• Molecular Formula: C₄₄H₃₉NO₁₁
• Molecular Weight: 757.794

Synonyms:N-fluorenylmethyloxycarbonyl-O-(2,3-di-O-benzoyl-β-D-xylopyranosyl)-L-serine benzyl ester

Chemical Property of N-fluorenylmethyloxycarbonyl-O-(2,3-di-O-benzoyl-β-D-xylopyranosyl)-L-serine benzyl ester

Chemical Property:

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Technology Process of N-fluorenylmethyloxycarbonyl-O-(2,3-di-O-benzoyl-β-D-xylopyranosyl)-L-serine benzyl ester

There total 24 articles about N-fluorenylmethyloxycarbonyl-O-(2,3-di-O-benzoyl-β-D-xylopyranosyl)-L-serine benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

N-fluorenylmethyloxycarbonyl-O-(2,3-di-O-benzoyl-4-O-p-methoxybenzyl-β-D-xylopyranosyl)-L-serine benzyl ester (1415218-11-9) → N-fluorenylmethyloxycarbonyl-O-(2,3-di-O-benzoyl-β-D-xylopyranosyl)-L-serine benzyl ester (1415218-13-1)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1002/anie.201205601

Reference yield: 80.0%

N-fluorenylmethyloxycarbonyl-O-(2,3-di-O-benzoyl-4-O-tert-butyldimethylsilyl-β-D-xylopyranosyl)-L-serine benzyl ester (1415218-12-0) → N-fluorenylmethyloxycarbonyl-O-(2,3-di-O-benzoyl-β-D-xylopyranosyl)-L-serine benzyl ester (1415218-13-1)

Guidance literature:

With trifluoromethylsulfonic anhydride; In dichloromethane; water; at 0 - 20 ℃; for 2h; Inert atmosphere;

DOI:10.1002/anie.201205601

Reference yield: 61.0%

N-fluorenylmethyloxycarbonyl-O-(2,3-di-O-benzoyl-4-O-benzyl-β-D-xylopyranosyl)-L-serine benzyl ester (1415218-10-8) → N-fluorenylmethyloxycarbonyl-O-(2,3-di-O-benzoyl-β-D-xylopyranosyl)-L-serine benzyl ester (1415218-13-1)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water; at 0 ℃; Reflux; Inert atmosphere;

DOI:10.1002/anie.201205601

upstream raw materials:

benzoyl chloride

benzyl bromide

D-Xylose

1,2,3,4-tetra-O-acetyl-D-xylopyranose

Downstream raw materials:

N-fluorenylmethyloxycarbonyl-O-[2-O-benzoyl-3-O-levulinoyl-4,6-O-benzylidene-β-D-galactopyranosyl-(1→4)-2,3-di-O-benzoyl-β-D-xylopyranosyl]-L-serine benzyl ester

N-fluorenylmethyloxycarbonyl-O-[2,3-di-O-levulinoyl-4,6-O-benzylidene-β-D-galactopyranosyl-(1→3)-2-O-benzoyl-4,6-O-benzylidene-β-D-galactopyranosyl-(1→4)-2,3-di-O-benzoyl-β-D-xylopyranosyl]-L-serine benzyl ester

N-fluorenylmethyloxycarbonyl-O-[2,3-di-O-levulinoyl-4,6-O-benzylidene-β-D-galactopyranosyl-(1→3)-2-O-benzoyl-4,6-O-benzylidene-α-D-galactopyranosyl-(1→4)-2,3-di-O-benzoyl-β-D-xylopyranosyl]-L-serine benzyl ester

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