biphenyl-2-ylcarbamic Acid 1-[2-(2-Chloro-4-formyl-5-methoxyphenylcarbamoyl)-ethyl]piperidin-4-yl Ester

Base Information

Chemical Name:biphenyl-2-ylcarbamic Acid 1-[2-(2-Chloro-4-formyl-5-methoxyphenylcarbamoyl)-ethyl]piperidin-4-yl Ester
CAS No.:743461-63-4
Molecular Formula:C₂₉H₃₀ClN₃O₅
Molecular Weight:536.027
Hs Code.:

Synonyms:biphenyl-2-ylcarbamic Acid 1-[2-(2-Chloro-4-formyl-5-methoxyphenylcarbamoyl)-ethyl]piperidin-4-yl Ester

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Chemical Property of biphenyl-2-ylcarbamic Acid 1-[2-(2-Chloro-4-formyl-5-methoxyphenylcarbamoyl)-ethyl]piperidin-4-yl Ester

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Technology Process of biphenyl-2-ylcarbamic Acid 1-[2-(2-Chloro-4-formyl-5-methoxyphenylcarbamoyl)-ethyl]piperidin-4-yl Ester

There total 12 articles about biphenyl-2-ylcarbamic Acid 1-[2-(2-Chloro-4-formyl-5-methoxyphenylcarbamoyl)-ethyl]piperidin-4-yl Ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 743461-62-3
biphenyl-2-ylcarbamic Acid 1-[2-(2-Chloro-4-hydroxymethyl-5-methoxy-phenylcarbamoyl)ethyl]piperidin-4-yl Ester

: 743461-63-4
biphenyl-2-ylcarbamic Acid 1-[2-(2-Chloro-4-formyl-5-methoxyphenylcarbamoyl)-ethyl]piperidin-4-yl Ester

Guidance literature:: With sulfur trioxide pyridine complex; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; In dichloromethane; at -20 - 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/jm501915g

Reference yield: 82.0%

: 1251456-87-7
N-(2-chloro-4-formyl-5-methoxyphenyl)acrylamide

: 171722-92-2
4-piperidyl N-(2-biphenyl)carbamate

: 743461-63-4
biphenyl-2-ylcarbamic Acid 1-[2-(2-Chloro-4-formyl-5-methoxyphenylcarbamoyl)-ethyl]piperidin-4-yl Ester

Guidance literature:: With acetic acid; In 2-methyltetrahydrofuran; at 60 - 75 ℃; for 2.08333h; Product distribution / selectivity; Industry scale;

Reference yield:

: 171722-92-2
4-piperidyl N-(2-biphenyl)carbamate

: 743461-63-4
biphenyl-2-ylcarbamic Acid 1-[2-(2-Chloro-4-formyl-5-methoxyphenylcarbamoyl)-ethyl]piperidin-4-yl Ester

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran; methanol / 16 h / 50 °C / Inert atmosphere

2: lithium borohydride / tetrahydrofuran; methanol / 0 - 20 °C / Inert atmosphere

3: N-ethyl-N,N-diisopropylamine; dimethyl sulfoxide; sulfur trioxide pyridine complex / dichloromethane / 0.5 h / -20 - 0 °C / Inert atmosphere

With lithium borohydride; sulfur trioxide pyridine complex; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jm501915g