(2R,3R)-tert-butyl 4-((2-chloropropyl)(4-methoxybenzyl)amino)-2,3-dihydroxy-4-oxobutanoate

Base Information

Chemical Name:(2R,3R)-tert-butyl 4-((2-chloropropyl)(4-methoxybenzyl)amino)-2,3-dihydroxy-4-oxobutanoate
CAS No.:1616239-00-9
Molecular Formula:C₁₉H₂₈ClNO₆
Molecular Weight:401.887
Hs Code.:

Synonyms:(2R,3R)-tert-butyl 4-((2-chloropropyl)(4-methoxybenzyl)amino)-2,3-dihydroxy-4-oxobutanoate

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Chemical Property of (2R,3R)-tert-butyl 4-((2-chloropropyl)(4-methoxybenzyl)amino)-2,3-dihydroxy-4-oxobutanoate

Chemical Property:

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Technology Process of (2R,3R)-tert-butyl 4-((2-chloropropyl)(4-methoxybenzyl)amino)-2,3-dihydroxy-4-oxobutanoate

There total 5 articles about (2R,3R)-tert-butyl 4-((2-chloropropyl)(4-methoxybenzyl)amino)-2,3-dihydroxy-4-oxobutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1616238-99-3
(2R,3R)-1-(tert-butoxy)-4-((2-chloropropyl)(4-methoxybenzyl)amino)-1,4-dioxobutane-2,3-diyl diacetate

: 1616239-00-9
(2R,3R)-tert-butyl 4-((2-chloropropyl)(4-methoxybenzyl)amino)-2,3-dihydroxy-4-oxobutanoate

Guidance literature:: With potassium cyanide; In methanol; at 0 ℃; for 4h; Inert atmosphere;

Reference yield:

: 856978-80-8
1-{[(4-methoxyphenyl)methyl]amino}propan-2-ol

: 1616239-00-9
(2R,3R)-tert-butyl 4-((2-chloropropyl)(4-methoxybenzyl)amino)-2,3-dihydroxy-4-oxobutanoate

Guidance literature:: Multi-step reaction with 4 steps

1: thionyl chloride / 1,2-dichloro-ethane / 4 h / 60 °C

2: tetrahydrofuran / 0 - 4 °C / Inert atmosphere

3: tetrahydrofuran / 5 h / 60 °C / Inert atmosphere

4: potassium cyanide / methanol / 4 h / 0 °C / Inert atmosphere

With potassium cyanide; thionyl chloride; In tetrahydrofuran; methanol; 1,2-dichloro-ethane;

Reference yield:

: 854304-10-2
2-chloro-N-(4-methoxybenzyl)propan-1-amine

: 1616239-00-9
(2R,3R)-tert-butyl 4-((2-chloropropyl)(4-methoxybenzyl)amino)-2,3-dihydroxy-4-oxobutanoate

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / 0 - 4 °C / Inert atmosphere

2: tetrahydrofuran / 5 h / 60 °C / Inert atmosphere

3: potassium cyanide / methanol / 4 h / 0 °C / Inert atmosphere

With potassium cyanide; In tetrahydrofuran; methanol;