C₂₀H₃₇⁽²⁾H₂NO₄Si

Base Information

Chemical Name:C₂₀H₃₇⁽²⁾H₂NO₄Si
CAS No.:1309572-15-3
Molecular Formula:C₂₀H₃₉NO₄Si
Molecular Weight:387.604
Hs Code.:

C<sub>20</sub>H<sub>37</sub><sup>(2)</sup>H<sub>2</sub>NO<sub>4</sub>Si

Synonyms:C₂₀H₃₇⁽²⁾H₂NO₄Si

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Chemical Property of C₂₀H₃₇⁽²⁾H₂NO₄Si

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Technology Process of C₂₀H₃₇⁽²⁾H₂NO₄Si

There total 8 articles about C₂₀H₃₇⁽²⁾H₂NO₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1330634-20-2
C₁₄H₂₃⁽²⁾H₂NO₄

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1309572-15-3
C₂₀H₃₇⁽²⁾H₂NO₄Si

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol201120k

Reference yield:

: C₂₆H₃₅NO₅

: 1309572-15-3
C₂₀H₃₇⁽²⁾H₂NO₄Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: diisobutylaluminium hydride / hexane; toluene / 2 h / -78 °C / Inert atmosphere

1.2: -78 - 20 °C

2.1: chromium dichloride; sodium iodide / tetrahydrofuran / 20 °C / Inert atmosphere

3.1: Grubbs catalyst first generation / dichloromethane / 20 °C / Inert atmosphere

4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C / Inert atmosphere

5.1: dmap; triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

With Grubbs catalyst first generation; chromium dichloride; dmap; sodium hydride; diisobutylaluminium hydride; triethylamine; sodium iodide; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; toluene; mineral oil; 2.1: Nozaki-Hiyama-Kishi reaction;
DOI:10.1021/ol201120k

Reference yield:

: (E)-2,3-dideuteroocta-2,7-dien-1-ol

: 1309572-15-3
C₂₀H₃₇⁽²⁾H₂NO₄Si

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine; dmap / dichloromethane / 0 - 20 °C / Inert atmosphere

2: chromium dichloride; sodium iodide / tetrahydrofuran / 20 °C / Inert atmosphere

3: Grubbs catalyst first generation / dichloromethane / 20 °C / Inert atmosphere

4: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C / Inert atmosphere

5: dmap; triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

With pyridine; Grubbs catalyst first generation; chromium dichloride; dmap; sodium hydride; triethylamine; sodium iodide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; mineral oil; 2: Nozaki-Hiyama-Kishi reaction;
DOI:10.1021/ol201120k