Technology Process of C43H58O10Si
There total 18 articles about C43H58O10Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dmap; triethylamine;
In
dichloromethane;
at 20 ℃;
DOI:10.1038/nchem.1074
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: potassium carbonate / methanol; water / 50 °C
1.2: 0 °C
2.1: 2,6-dimethylpyridine; trifluoromethylsulfonic anhydride / dichloromethane / -78 °C
2.2: 65 °C
3.1: ammonium chloride; zinc / ethanol / 160 °C / Microwave irradiation
4.1: pyridinium p-toluenesulfonate / dichloromethane / 40 °C
5.1: N-Bromosuccinimide; sodium hydrogencarbonate; dibenzoyl peroxide / tetrachloromethane; benzene / 70 °C
5.2: 20 °C
6.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C
7.1: dmap; triethylamine / dichloromethane / 20 °C
With
2,6-dimethylpyridine; dmap; N-Bromosuccinimide; lithium aluminium tetrahydride; trifluoromethylsulfonic anhydride; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; potassium carbonate; ammonium chloride; triethylamine; zinc; dibenzoyl peroxide;
In
tetrahydrofuran; methanol; tetrachloromethane; ethanol; dichloromethane; water; benzene;
DOI:10.1038/nchem.1074
- Guidance literature:
-
Multi-step reaction with 9 steps
1.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 20 °C
2.1: cerium(III) chloride / tetrahydrofuran / -78 °C
3.1: potassium carbonate / methanol; water / 50 °C
3.2: 0 °C
4.1: 2,6-dimethylpyridine; trifluoromethylsulfonic anhydride / dichloromethane / -78 °C
4.2: 65 °C
5.1: ammonium chloride; zinc / ethanol / 160 °C / Microwave irradiation
6.1: pyridinium p-toluenesulfonate / dichloromethane / 40 °C
7.1: N-Bromosuccinimide; sodium hydrogencarbonate; dibenzoyl peroxide / tetrachloromethane; benzene / 70 °C
7.2: 20 °C
8.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C
9.1: dmap; triethylamine / dichloromethane / 20 °C
With
2,6-dimethylpyridine; dmap; N-Bromosuccinimide; lithium aluminium tetrahydride; cerium(III) chloride; trifluoromethylsulfonic anhydride; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; potassium carbonate; ammonium chloride; Dess-Martin periodane; triethylamine; zinc; dibenzoyl peroxide;
In
tetrahydrofuran; methanol; tetrachloromethane; ethanol; dichloromethane; water; benzene;
DOI:10.1038/nchem.1074