(S_S,3R)-(+)-methyl 3-[N-(p-toluenesulfinyl)amino]-3-(phenyl)propanoate

Base Information

Chemical Name:(S_S,3R)-(+)-methyl 3-[N-(p-toluenesulfinyl)amino]-3-(phenyl)propanoate
CAS No.:158009-86-0
Molecular Formula:C₁₇H₁₉NO₃S
Molecular Weight:317.409
Hs Code.:

(S<sub>S</sub>,3R)-(+)-methyl 3-[N-(p-toluenesulfinyl)amino]-3-(phenyl)propanoate

Synonyms:(S_S,3R)-(+)-methyl 3-[N-(p-toluenesulfinyl)amino]-3-(phenyl)propanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S_S,3R)-(+)-methyl 3-[N-(p-toluenesulfinyl)amino]-3-(phenyl)propanoate

Chemical Property:

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Technology Process of (S_S,3R)-(+)-methyl 3-[N-(p-toluenesulfinyl)amino]-3-(phenyl)propanoate

There total 6 articles about (S_S,3R)-(+)-methyl 3-[N-(p-toluenesulfinyl)amino]-3-(phenyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 79-20-9
acetic acid methyl ester

: 350479-90-2
(S,E)-N-benzylidene-4-methylbenzenesulfinamide

: 158009-86-0
(S_S,3R)-(+)-methyl 3-[N-(p-toluenesulfinyl)amino]-3-(phenyl)propanoate

: 267011-72-3
methyl (S_S,R)-(+)-methyl 3-oxo-5-phenyl-5-(p-toluenesulfinylamino)pentanoate

Guidance literature:: With sodium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 3.5h;
DOI:10.1021/ol005580j

Reference yield: 84.0%

: 79-20-9
acetic acid methyl ester

: 350479-90-2
(S,E)-N-benzylidene-4-methylbenzenesulfinamide

: 158009-86-0
(S_S,3R)-(+)-methyl 3-[N-(p-toluenesulfinyl)amino]-3-(phenyl)propanoate

Guidance literature:: With sodium hexamethyldisilazane; In tetrahydrofuran; diethyl ether; 1.) -78 deg C, 40 min, 2.) -78 deg C, 7 h;
DOI:10.1021/jo00126a070

Reference yield:

: 79-20-9
acetic acid methyl ester

: 153277-49-7
(S)-N-benzylidene-4-toluenesulfinamide

: C₁₇H₁₉NO₃S

: 158009-86-0
(S_S,3R)-(+)-methyl 3-[N-(p-toluenesulfinyl)amino]-3-(phenyl)propanoate

Guidance literature:: acetic acid methyl ester; With potassium hexamethylsilazane; In tetrahydrofuran; at -78 ℃; for 0.75h;

(S)-N-benzylidene-4-toluenesulfinamide; In tetrahydrofuran; at -78 ℃; for 9h; Overall yield = 68 %;
DOI:10.1039/c5ob01140j