(1R,2S,3R,4S)-1-<(methoxycarbonyl)amino>-2,3-<(dimethylmethylene)dioxy>-4-<(phenylseleno)methyl>cyclopentane

Base Information

Chemical Name:(1R,2S,3R,4S)-1-<(methoxycarbonyl)amino>-2,3-<(dimethylmethylene)dioxy>-4-<(phenylseleno)methyl>cyclopentane
CAS No.:84955-52-2
Molecular Formula:C₁₇H₂₃NO₄Se
Molecular Weight:384.334
Hs Code.:

Synonyms:(1R,2S,3R,4S)-1-<(methoxycarbonyl)amino>-2,3-<(dimethylmethylene)dioxy>-4-<(phenylseleno)methyl>cyclopentane

Suppliers and Price of (1R,2S,3R,4S)-1-<(methoxycarbonyl)amino>-2,3-<(dimethylmethylene)dioxy>-4-<(phenylseleno)methyl>cyclopentane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,2S,3R,4S)-1-<(methoxycarbonyl)amino>-2,3-<(dimethylmethylene)dioxy>-4-<(phenylseleno)methyl>cyclopentane

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Technology Process of (1R,2S,3R,4S)-1-<(methoxycarbonyl)amino>-2,3-<(dimethylmethylene)dioxy>-4-<(phenylseleno)methyl>cyclopentane

There total 8 articles about (1R,2S,3R,4S)-1-<(methoxycarbonyl)amino>-2,3-<(dimethylmethylene)dioxy>-4-<(phenylseleno)methyl>cyclopentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 85026-58-0
(1R,5R,6R,7S)-6,7-(isopropylidenedioxy)-3-oxabicyclo[3.2.1]octane-2-one

: 84955-52-2
(1R,2S,3R,4S)-1-<(methoxycarbonyl)amino>-2,3-<(dimethylmethylene)dioxy>-4-<(phenylseleno)methyl>cyclopentane

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / NaBH₄ / dimethylformamide / 2 h / 120 °C

2: 1.) triethylamine, ethyl chloroformate, 2.) NaN₃

With sodium tetrahydroborate; sodium azide; chloroformic acid ethyl ester; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1021/ja00350a050

Reference yield:

: 1666-13-3
diphenyl diselenide

: 84955-52-2
(1R,2S,3R,4S)-1-<(methoxycarbonyl)amino>-2,3-<(dimethylmethylene)dioxy>-4-<(phenylseleno)methyl>cyclopentane

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / NaBH₄ / dimethylformamide / 2 h / 120 °C

2: 1.) triethylamine, ethyl chloroformate, 2.) NaN₃

With sodium tetrahydroborate; sodium azide; chloroformic acid ethyl ester; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1021/ja00350a050

Reference yield:

: 84955-44-2
(3aS,4R,6R,6aR)-6-Hydroxymethyl-2,2-dimethyl-tetrahydro-cyclopenta[1,3]dioxole-4-carboxylic acid

: 84955-52-2
(1R,2S,3R,4S)-1-<(methoxycarbonyl)amino>-2,3-<(dimethylmethylene)dioxy>-4-<(phenylseleno)methyl>cyclopentane

Guidance literature:: Multi-step reaction with 3 steps

1: 968 mg / acetic anhydride, pyridine / Ambient temperature

2: 93 percent / NaBH₄ / dimethylformamide / 2 h / 120 °C

3: 1.) triethylamine, ethyl chloroformate, 2.) NaN₃

With pyridine; sodium tetrahydroborate; sodium azide; chloroformic acid ethyl ester; acetic anhydride; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1021/ja00350a050