1-(4'-chloroacetylamino)phenyl-1,4-dihydro-3(2H)-benzoisoquinolinone

Base Information

Chemical Name:1-(4'-chloroacetylamino)phenyl-1,4-dihydro-3(2H)-benzoisoquinolinone
CAS No.:81250-67-1
Molecular Formula:C₂₁H₁₇ClN₂O₂
Molecular Weight:364.831
Hs Code.:

1-(4'-chloroacetylamino)phenyl-1,4-dihydro-3(2H)-benzo<h>isoquinolinone

Synonyms:1-(4'-chloroacetylamino)phenyl-1,4-dihydro-3(2H)-benzoisoquinolinone

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Chemical Property of 1-(4'-chloroacetylamino)phenyl-1,4-dihydro-3(2H)-benzoisoquinolinone

Chemical Property:

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Technology Process of 1-(4'-chloroacetylamino)phenyl-1,4-dihydro-3(2H)-benzoisoquinolinone

There total 4 articles about 1-(4'-chloroacetylamino)phenyl-1,4-dihydro-3(2H)-benzoisoquinolinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.9%

: 81250-60-4
1-(4'-aminophenyl)-1,4-dihydro-3(2H)-benzoisoquinolinone

: 79-04-9
chloroacetyl chloride

: 81250-67-1
1-(4'-chloroacetylamino)phenyl-1,4-dihydro-3(2H)-benzoisoquinolinone

Guidance literature:: With triethylamine; In acetic acid; at 55 ℃; for 6h;

Reference yield:

: 7498-57-9
2-naphthaleneacetonitrile

: 81250-67-1
1-(4'-chloroacetylamino)phenyl-1,4-dihydro-3(2H)-benzoisoquinolinone

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) polyphosphoric acid / 1.) water, 90 degC, 30 min; 2.) 120 degC, 3 h

2: 57.3 percent / 10percent Engelhardt catalyst / dimethylformamide

3: 69.9 percent / triethylamine / acetic acid / 6 h / 55 °C

With PPA; triethylamine; palladium on activated charcoal; In acetic acid; N,N-dimethyl-formamide;

Reference yield:

: 555-16-8
4-nitrobenzaldehdye

: 81250-67-1
1-(4'-chloroacetylamino)phenyl-1,4-dihydro-3(2H)-benzoisoquinolinone

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) polyphosphoric acid / 1.) water, 90 degC, 30 min; 2.) 120 degC, 3 h

2: 57.3 percent / 10percent Engelhardt catalyst / dimethylformamide

3: 69.9 percent / triethylamine / acetic acid / 6 h / 55 °C

With PPA; triethylamine; palladium on activated charcoal; In acetic acid; N,N-dimethyl-formamide;