bis(ethyl 3-oxo-3-phenylpropanoato)zirconium(IV) phthalocyanine

Base Information

• Chemical Name: bis(ethyl 3-oxo-3-phenylpropanoato)zirconium(IV) phthalocyanine
• CAS No.: 935658-54-1
• Molecular Formula: C₅₄H₃₈N₈O₆Zr
• Molecular Weight: 986.17
• Mol file: 935658-54-1.mol

Synonyms:bis(ethyl 3-oxo-3-phenylpropanoato)zirconium(IV) phthalocyanine

Chemical Property of bis(ethyl 3-oxo-3-phenylpropanoato)zirconium(IV) phthalocyanine

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of bis(ethyl 3-oxo-3-phenylpropanoato)zirconium(IV) phthalocyanine

There total 2 articles about bis(ethyl 3-oxo-3-phenylpropanoato)zirconium(IV) phthalocyanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

dihydroxy(phthalocyaninato)zirconium(IV) (423176-27-6,71817-74-8) + (E)-1-ethoxy-3-oxo-3-phenylprop-1-en-1-ol → bis(ethyl 3-oxo-3-phenylpropanoato)zirconium(IV) phthalocyanine (935658-54-1)

Guidance literature:

In toluene; for 3h; Heating;

DOI:10.1134/S0036023620100046

Reference yield: 25.0%

dichloro(phthalocyaninato)zirconium(IV) (59538-92-0) + ethyl 3-oxo-3-phenylpropionate (94-02-0) → bis(ethyl 3-oxo-3-phenylpropanoato)zirconium(IV) phthalocyanine (935658-54-1)

Guidance literature:

In toluene; byproducts: HCl; metal compd. (0.74 mmol) suspnd., ligand (1.67 mmol) added, refluxed for3-5 h at 116°C; filtered while hot, hexane added, crystd. on cooling, septd., washed (hexane), dried in air, dried (vac., 60°C, 8 h), elem. anal.;

DOI:10.1016/j.ica.2006.08.035

upstream raw materials:

dichloro(phthalocyaninato)zirconium(IV)

ethyl 3-oxo-3-phenylpropionate

dihydroxy(phthalocyaninato)zirconium(IV)