C₃₀H₃₆N₄O₆

Base Information

Chemical Name:C₃₀H₃₆N₄O₆
CAS No.:1093190-00-1
Molecular Formula:C₃₀H₃₆N₄O₆
Molecular Weight:548.639
Hs Code.:

C<sub>30</sub>H<sub>36</sub>N<sub>4</sub>O<sub>6</sub>

Synonyms:C₃₀H₃₆N₄O₆

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Chemical Property of C₃₀H₃₆N₄O₆

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Technology Process of C₃₀H₃₆N₄O₆

There total 8 articles about C₃₀H₃₆N₄O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.8%

: 1093189-99-1
C₃₁H₃₇N₃O₆

: 1093190-00-1
C₃₀H₃₆N₄O₆

Guidance literature:: C₃₁H₃₇N₃O₆; With sodium hydroxide; hydroxylamine hydrochloride; In methanol; dichloromethane; at 20 ℃; for 72h;

With water; ammonium chloride; In methanol; dichloromethane; pH=7;

Reference yield:

: 16004-15-2
1-bromomethyl-4-iodobenzene

: 1093190-00-1
C₃₀H₃₆N₄O₆

Guidance literature:: Multi-step reaction with 7 steps

1.1: dimethyl sulfoxide / 20 °C

2.1: copper(l) iodide; triethylamine / bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran / 0 - 20 °C

3.1: Dess-Martin periodane / dichloromethane / 0 - 20 °C

4.1: sodium hydride / tetrahydrofuran / 1 h / 20 °C

4.2: 20 °C

5.1: sodium hydroxide / methanol / 4 h / Heating / reflux

5.2: pH 7

6.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

7.1: sodium hydroxide; hydroxylamine hydrochloride / methanol; dichloromethane / 72 h / 20 °C

7.2: pH 7

With sodium hydroxide; copper(l) iodide; hydroxylamine hydrochloride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; sodium hydride; Dess-Martin periodane; triethylamine; N-ethyl-N,N-diisopropylamine; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 15164-44-0
p-(iodophenyl)carboxaldehyde

: 1093190-00-1
C₃₀H₃₆N₄O₆

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium tris(acetoxy)borohydride / tetrahydrofuran / 0 - 20 °C

2.1: copper(l) iodide; triethylamine / bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran / 0 - 20 °C

3.1: Dess-Martin periodane / dichloromethane / 0 - 20 °C

4.1: sodium hydride / tetrahydrofuran / 1 h / 20 °C

4.2: 20 °C

5.1: sodium hydroxide / methanol / 4 h / Heating / reflux

5.2: pH 7

6.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

7.1: sodium hydroxide; hydroxylamine hydrochloride / methanol; dichloromethane / 72 h / 20 °C

7.2: pH 7

With sodium hydroxide; copper(l) iodide; hydroxylamine hydrochloride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; sodium tris(acetoxy)borohydride; sodium hydride; Dess-Martin periodane; triethylamine; N-ethyl-N,N-diisopropylamine; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;