1-<6-(benzyloxycarbonylamino)hexyl>-4-methyl-3-phenacylimidazolium iodide

Base Information

Chemical Name:1-<6-(benzyloxycarbonylamino)hexyl>-4-methyl-3-phenacylimidazolium iodide
CAS No.:115375-00-3
Molecular Formula:C₂₆H₃₂N₃O₃*I
Molecular Weight:561.463
Hs Code.:

Synonyms:1-<6-(benzyloxycarbonylamino)hexyl>-4-methyl-3-phenacylimidazolium iodide

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Chemical Property of 1-<6-(benzyloxycarbonylamino)hexyl>-4-methyl-3-phenacylimidazolium iodide

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Technology Process of 1-<6-(benzyloxycarbonylamino)hexyl>-4-methyl-3-phenacylimidazolium iodide

There total 3 articles about 1-<6-(benzyloxycarbonylamino)hexyl>-4-methyl-3-phenacylimidazolium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 51224-11-4
6-(benzyloxycarbonylamino)-1-iodohexane

: 115374-99-7
5-methyl-1-phenacylimidazole

: 115375-00-3
1-<6-(benzyloxycarbonylamino)hexyl>-4-methyl-3-phenacylimidazolium iodide

Guidance literature:: In chloroform; for 28h; Heating;
DOI:10.1055/s-1987-28187

Reference yield:

: 115383-28-3
4-methyl-3-phenacyl-1-triphenylmethylimidazolium bromide

: 115375-00-3
1-<6-(benzyloxycarbonylamino)hexyl>-4-methyl-3-phenacylimidazolium iodide

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / 50percent aq. AcOH / 0.25 h / Heating

2: 88 percent / CHCl₃ / 28 h / Heating

With acetic acid; In chloroform;
DOI:10.1055/s-1987-28187

Reference yield:

: 70-11-1
α-bromoacetophenone

: 115375-00-3
1-<6-(benzyloxycarbonylamino)hexyl>-4-methyl-3-phenacylimidazolium iodide

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / CH₂Cl₂; diethyl ether / 48 h / Ambient temperature

2: 84 percent / 50percent aq. AcOH / 0.25 h / Heating

3: 88 percent / CHCl₃ / 28 h / Heating

With acetic acid; In diethyl ether; dichloromethane; chloroform;
DOI:10.1055/s-1987-28187