(R)-2-(4-hydroxy-4-methylpiperidin-1-yl)-2-phenylacetic acid trifluoroacetic acid salt

Base Information

Chemical Name:(R)-2-(4-hydroxy-4-methylpiperidin-1-yl)-2-phenylacetic acid trifluoroacetic acid salt
CAS No.:1007878-29-6
Molecular Formula:C₂HF₃O₂*C₁₄H₁₉NO₃
Molecular Weight:363.334
Hs Code.:

Synonyms:(R)-2-(4-hydroxy-4-methylpiperidin-1-yl)-2-phenylacetic acid trifluoroacetic acid salt

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Chemical Property of (R)-2-(4-hydroxy-4-methylpiperidin-1-yl)-2-phenylacetic acid trifluoroacetic acid salt

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Technology Process of (R)-2-(4-hydroxy-4-methylpiperidin-1-yl)-2-phenylacetic acid trifluoroacetic acid salt

There total 5 articles about (R)-2-(4-hydroxy-4-methylpiperidin-1-yl)-2-phenylacetic acid trifluoroacetic acid salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1007878-24-1
(S)-1-phenylethyl (R)-2-(4-hydroxy-4-methylpiperidin-1-yl)-2-phenylacetate

: 1007878-29-6
(R)-2-(4-hydroxy-4-methylpiperidin-1-yl)-2-phenylacetic acid trifluoroacetic acid salt

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 2h;

Reference yield: 98.0%

: 1007878-24-1
(S)-1-phenylethyl (R)-2-(4-hydroxy-4-methylpiperidin-1-yl)-2-phenylacetate

: 76-05-1
trifluoroacetic acid

: 1007878-29-6
(R)-2-(4-hydroxy-4-methylpiperidin-1-yl)-2-phenylacetic acid trifluoroacetic acid salt

Guidance literature:: In dichloromethane; at 20 ℃; for 2h;

Reference yield:

: 1007878-22-9
(S)-1-phenylethyl 2-bromo-2-phenylacetate

: 1007878-29-6
(R)-2-(4-hydroxy-4-methylpiperidin-1-yl)-2-phenylacetic acid trifluoroacetic acid salt

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine; tetra-(n-butyl)ammonium iodide / tetrahydrofuran / 0.08 h / 20 °C

1.2: 5 h / 20 - 60 °C

2.1: dichloromethane / 2 h / 20 °C

With tetra-(n-butyl)ammonium iodide; triethylamine; In tetrahydrofuran; dichloromethane;