2-Chloro-4-methoxybenzene-1-sulfonyl chloride

Base Information

• Chemical Name: 2-Chloro-4-methoxybenzene-1-sulfonyl chloride
• CAS No.: 23094-94-2
• Molecular Formula: C₇H₆Cl₂O₃S
• Molecular Weight: 241.095
• European Community (EC) Number: 828-614-1

Synonyms:2-CHLORO-4-METHOXYBENZENE-1-SULFONYL CHLORIDE;23094-94-2;2-chloro-4-methoxybenzenesulfonyl chloride;SCHEMBL1817972;KVRCCIGDMLSANW-UHFFFAOYSA-N;AKOS000155411;DB-192656;CS-0214914;C80021;EN300-204251;2-CHLORO-4-METHOXYBENZENE-1-SULFONYLCHLORIDE

Chemical Property of 2-Chloro-4-methoxybenzene-1-sulfonyl chloride

Chemical Property:

• XLogP3: 2.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 239.9414706
• Heavy Atom Count: 13
• Complexity: 259

Purity/Quality:

99% ^*data from raw suppliers

2-CHLORO-4-METHOXYBENZENE-1-SULFONYL CHLORIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: COC1=CC(=C(C=C1)S(=O)(=O)Cl)Cl

Technology Process of 2-Chloro-4-methoxybenzene-1-sulfonyl chloride

There total 1 articles about 2-Chloro-4-methoxybenzene-1-sulfonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-chloro-3-methoxy-benzene (2845-89-8) → 2-chloro-4-methoxybenzenesulfonyl chloride (23094-94-2)

Guidance literature:

With chlorosulfonic acid;

DOI:10.1039/j39690001341

Reference yield: 64.0%

4,5-dihydro-2-[4-[[methyl[[2-(methylamino)ethoxy]acetyl]amino]methyl]phenyl]-1H-imidazole-1-carboxylic acid 1,1-dimethylethyl ester (633698-75-6) + 2-chloro-4-methoxybenzenesulfonyl chloride (23094-94-2) → 2-[4-[[[[2-[[(2-chloro-4-methoxyphenyl)sulfonyl]methylamino]ethoxy]acetyl]methylamino]methyl]phenyl]-4,5-dihydro-1H-imidazole-1-carboxylic acid 1,1-dimethylethyl ester

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1021/jm2016057

Reference yield:

2-chloro-4-methoxybenzenesulfonyl chloride (23094-94-2) + ethyl bromoacetate (105-36-2) → C11H13ClO5S (1117877-52-7)

Guidance literature:

With ammonium chloride; zinc; In tetrahydrofuran; at 110 ℃;

DOI:10.1016/j.bmcl.2008.11.026

upstream raw materials:

1-chloro-3-methoxy-benzene

Downstream raw materials:

2-Chlor-4-methoxy-benzolsulfonsaeure-isopropylidenhydrazid

C₁₁H₁₃ClO₅S

2-chloro-4-hydroxy-N,N-dimethylbenzenesulfonamide

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