3-Methyl-5-phenyl-1,6,6aλ⁴-trithia-3-azacyclopentapentalen-4(3H)-thion

Base Information

Chemical Name:3-Methyl-5-phenyl-1,6,6aλ⁴-trithia-3-azacyclopentapentalen-4(3H)-thion
CAS No.:139102-07-1
Molecular Formula:C₁₃H₉NS₄
Molecular Weight:307.485
Hs Code.:

3-Methyl-5-phenyl-1,6,6aλ<sup>4</sup>-trithia-3-azacyclopenta<c,d>pentalen-4(3H)-thion

Synonyms:3-Methyl-5-phenyl-1,6,6aλ⁴-trithia-3-azacyclopentapentalen-4(3H)-thion

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Chemical Property of 3-Methyl-5-phenyl-1,6,6aλ⁴-trithia-3-azacyclopentapentalen-4(3H)-thion

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Technology Process of 3-Methyl-5-phenyl-1,6,6aλ⁴-trithia-3-azacyclopentapentalen-4(3H)-thion

There total 8 articles about 3-Methyl-5-phenyl-1,6,6aλ⁴-trithia-3-azacyclopentapentalen-4(3H)-thion which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 139102-04-8
6-Benzoyl-4-methyl-1,2-dithiolo<4,3-b>pyrrol-5(4H)-on

: 139102-07-1
3-Methyl-5-phenyl-1,6,6aλ⁴-trithia-3-azacyclopentapentalen-4(3H)-thion

Guidance literature:: With 2,4-bis(4-ethylthio)-2,4-dithioxo-1,3,2λ⁵,4λ⁵-dithiadiphosphetane; In toluene; at 100 ℃; for 2h;

Reference yield:

: 98-88-4
benzoyl chloride

: 139102-07-1
3-Methyl-5-phenyl-1,6,6aλ⁴-trithia-3-azacyclopentapentalen-4(3H)-thion

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / AlCl₃ / chlorobenzene / 2 h / 80 °C

2: 59 percent / Br₂ / acetic acid; CH₂Cl₂ / 24 h / Ambient temperature

3: 81 percent / 2,4-bis(ethylthio)-1,3,2,4-dithiadiphosphetan-2,4-dithione / toluene / 2 h / 100 °C

With aluminium trichloride; bromine; 2,4-bis(4-ethylthio)-2,4-dithioxo-1,3,2λ⁵,4λ⁵-dithiadiphosphetane; In dichloromethane; acetic acid; chlorobenzene; toluene;

Reference yield:

: 139101-96-5
5-Methyl-2,2-diphenyl-1,3-dithiino<5,4-b>pyrrol-6(5H)-on

: 139102-07-1
3-Methyl-5-phenyl-1,6,6aλ⁴-trithia-3-azacyclopentapentalen-4(3H)-thion

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / AlCl₃ / chlorobenzene / 2 h / 80 °C

2: 59 percent / Br₂ / acetic acid; CH₂Cl₂ / 24 h / Ambient temperature

3: 81 percent / 2,4-bis(ethylthio)-1,3,2,4-dithiadiphosphetan-2,4-dithione / toluene / 2 h / 100 °C

With aluminium trichloride; bromine; 2,4-bis(4-ethylthio)-2,4-dithioxo-1,3,2λ⁵,4λ⁵-dithiadiphosphetane; In dichloromethane; acetic acid; chlorobenzene; toluene;