1,2-undecadienyl phenyl sulfoxide

Base Information

• Chemical Name: 1,2-undecadienyl phenyl sulfoxide
• CAS No.: 527706-26-9
• Molecular Formula: C₁₇H₂₄OS
• Molecular Weight: 276.443
• Mol file: 527706-26-9.mol

Synonyms:1,2-undecadienyl phenyl sulfoxide

Chemical Property of 1,2-undecadienyl phenyl sulfoxide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,2-undecadienyl phenyl sulfoxide

There total 1 articles about 1,2-undecadienyl phenyl sulfoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

undec-1-yn-3-ol (53735-49-2) + benzenesulfenyl chloride (931-59-9) → 1,2-undecadienyl phenyl sulfoxide (527706-26-9)

Guidance literature:

undec-1-yn-3-ol; With triethylamine; In dichloromethane; at -85 ℃; for 0.166667h;

benzenesulfenyl chloride; In dichloromethane; at -85 - 20 ℃;

DOI:10.1021/ja034039q

Reference yield: 98.0%

1,2-undecadienyl phenyl sulfoxide (527706-26-9) → (E)-2-bromo-1-(phenylsulfinyl)-1-undecen-3-ol

Guidance literature:

With N-Bromosuccinimide; lithium acetate; In acetonitrile; at 20 ℃; for 2h;

DOI:10.1021/ja034039q

Reference yield: 89.0%

1,2-undecadienyl phenyl sulfoxide (527706-26-9) → (E)-2-iodo-1-(phenylsulfinyl)-1-undecen-3-ol (527706-82-7)

Guidance literature:

With lithium acetate; iodine; In acetonitrile; at 20 ℃; for 1h;

DOI:10.1021/ja034039q

upstream raw materials:

undec-1-yn-3-ol

benzenesulfenyl chloride

Downstream raw materials:

(E)-2-iodo-1-(phenylsulfinyl)-1-undecen-3-ol

Z-1-(benzenesulfinyl)-2-phenylundec-1-en-3-ol

Z-1-(benzenesulfonyl)-2-phenylundec-1-en-3-ol

(E)-2-iodo-1-phenylthio-1-undecen-3-ol