2-morpholinoethyl 4-(4-(4-(2-(hydroxyamino)-2-oxoethyl)phenyl)butyl)phenylcarbamate

Base Information

Chemical Name:2-morpholinoethyl 4-(4-(4-(2-(hydroxyamino)-2-oxoethyl)phenyl)butyl)phenylcarbamate
CAS No.:1579294-90-8
Molecular Formula:C₂₅H₃₃N₃O₅
Molecular Weight:455.554
Hs Code.:

Synonyms:2-morpholinoethyl 4-(4-(4-(2-(hydroxyamino)-2-oxoethyl)phenyl)butyl)phenylcarbamate

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Chemical Property of 2-morpholinoethyl 4-(4-(4-(2-(hydroxyamino)-2-oxoethyl)phenyl)butyl)phenylcarbamate

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Technology Process of 2-morpholinoethyl 4-(4-(4-(2-(hydroxyamino)-2-oxoethyl)phenyl)butyl)phenylcarbamate

There total 5 articles about 2-morpholinoethyl 4-(4-(4-(2-(hydroxyamino)-2-oxoethyl)phenyl)butyl)phenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 3.0%

: 1579295-43-4
C₂₆H₃₄N₂O₅

: 1579294-90-8
2-morpholinoethyl 4-(4-(4-(2-(hydroxyamino)-2-oxoethyl)phenyl)butyl)phenylcarbamate

Guidance literature:: With hydroxylamine; sodium methylate; In methanol; water; at 0 - 20 ℃; for 2h;

Reference yield:

: 1579295-40-1
methyl 2-(4-(4-(4-nitrophenyl)but-3-ynyl)phenyl)acetate

: 1579294-90-8
2-morpholinoethyl 4-(4-(4-(2-(hydroxyamino)-2-oxoethyl)phenyl)butyl)phenylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 21 h

2.1: pyridine / N,N-dimethyl-formamide / 1 h / 0 °C

2.2: 48 h / 60 °C

3.1: sodium methylate; hydroxylamine / methanol; water / 2 h / 0 - 20 °C

With pyridine; palladium 10% on activated carbon; hydrogen; hydroxylamine; sodium methylate; In methanol; water; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 1579295-41-2
methyl 2-(4-(4-(4-aminophenyl)butyl)phenyl)acetate

: 1579294-90-8
2-morpholinoethyl 4-(4-(4-(2-(hydroxyamino)-2-oxoethyl)phenyl)butyl)phenylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine / N,N-dimethyl-formamide / 1 h / 0 °C

1.2: 48 h / 60 °C

2.1: sodium methylate; hydroxylamine / methanol; water / 2 h / 0 - 20 °C

With pyridine; hydroxylamine; sodium methylate; In methanol; water; N,N-dimethyl-formamide;