N,N′-(6,6′-(2,3-dihydroxybutane-1,4-diyl)bis(oxy)bis-(5-(2-methoxyphenoxy)-2,2′-bipyrimidine-6,4-diyl))bis-(4-tert-butylbenzenesulfonamide)

Base Information

Chemical Name:N,N′-(6,6′-(2,3-dihydroxybutane-1,4-diyl)bis(oxy)bis-(5-(2-methoxyphenoxy)-2,2′-bipyrimidine-6,4-diyl))bis-(4-tert-butylbenzenesulfonamide)
CAS No.:1448588-53-1
Molecular Formula:C₅₄H₅₆N₁₀O₁₂S₂
Molecular Weight:1101.23
Hs Code.:

Synonyms:N,N′-(6,6′-(2,3-dihydroxybutane-1,4-diyl)bis(oxy)bis-(5-(2-methoxyphenoxy)-2,2′-bipyrimidine-6,4-diyl))bis-(4-tert-butylbenzenesulfonamide)

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Chemical Property of N,N′-(6,6′-(2,3-dihydroxybutane-1,4-diyl)bis(oxy)bis-(5-(2-methoxyphenoxy)-2,2′-bipyrimidine-6,4-diyl))bis-(4-tert-butylbenzenesulfonamide)

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Technology Process of N,N′-(6,6′-(2,3-dihydroxybutane-1,4-diyl)bis(oxy)bis-(5-(2-methoxyphenoxy)-2,2′-bipyrimidine-6,4-diyl))bis-(4-tert-butylbenzenesulfonamide)

There total 4 articles about N,N′-(6,6′-(2,3-dihydroxybutane-1,4-diyl)bis(oxy)bis-(5-(2-methoxyphenoxy)-2,2′-bipyrimidine-6,4-diyl))bis-(4-tert-butylbenzenesulfonamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1448588-52-0
N,N′-(6,6′-(2,2-dimethyl-1,3-dioxolane-4,5-diyl)bis-(methylene)bis(oxy)bis(5-(2-methoxy phenoxy)-2,2′-bipyrimidine-6,4-diyl))bis(4-tert-butylbenzenesulfonamide)

: 1448588-53-1
N,N′-(6,6′-(2,3-dihydroxybutane-1,4-diyl)bis(oxy)bis-(5-(2-methoxyphenoxy)-2,2′-bipyrimidine-6,4-diyl))bis-(4-tert-butylbenzenesulfonamide)

Guidance literature:: With hydrogenchloride; In acetonitrile;
DOI:10.1021/op400100s

Reference yield:

: 150727-06-3
4-tert-butyl-N-(6-chloro-5-(2-methoxyphenoxy)2,2'-bipyrimidin-4-yl)benzene sulfonamide

: 1448588-53-1
N,N′-(6,6′-(2,3-dihydroxybutane-1,4-diyl)bis(oxy)bis-(5-(2-methoxyphenoxy)-2,2′-bipyrimidine-6,4-diyl))bis-(4-tert-butylbenzenesulfonamide)

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / acetonitrile / 4 h / 80 - 85 °C

1.2: 14 h / 80 - 85 °C

2.1: hydrogenchloride / acetonitrile

With hydrogenchloride; sodium hydroxide; In acetonitrile;
DOI:10.1021/op400100s

Reference yield:

: 6292-59-7
4-tert-butylbenzenesulphonamide

: 1448588-53-1
N,N′-(6,6′-(2,3-dihydroxybutane-1,4-diyl)bis(oxy)bis-(5-(2-methoxyphenoxy)-2,2′-bipyrimidine-6,4-diyl))bis-(4-tert-butylbenzenesulfonamide)

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / toluene / 0.5 h / 50 °C / Large scale

1.2: 10 h / 110 °C / Large scale

2.1: sodium hydroxide / acetonitrile / 4 h / 80 - 85 °C

2.2: 14 h / 80 - 85 °C

3.1: hydrogenchloride / acetonitrile

With hydrogenchloride; potassium carbonate; sodium hydroxide; In toluene; acetonitrile;
DOI:10.1021/op400100s