N,N′-(6,6′-(2,2-dimethyl-1,3-dioxolane-4,5-diyl)bis-(methylene)bis(oxy)bis(5-(2-methoxy phenoxy)-2,2′-bipyrimidine-6,4-diyl))bis(4-tert-butylbenzenesulfonamide)

Base Information

Chemical Name:N,N′-(6,6′-(2,2-dimethyl-1,3-dioxolane-4,5-diyl)bis-(methylene)bis(oxy)bis(5-(2-methoxy phenoxy)-2,2′-bipyrimidine-6,4-diyl))bis(4-tert-butylbenzenesulfonamide)
CAS No.:1448588-52-0
Molecular Formula:C₅₇H₆₀N₁₀O₁₂S₂
Molecular Weight:1141.3
Hs Code.:

N,N′-(6,6′-(2,2-dimethyl-1,3-dioxolane-4,5-diyl)bis-(methylene)bis(oxy)bis(5-(2-methoxy phenoxy)-2,2′-bipyrimidine-6,4-diyl))bis(4-tert-butylbenzenesulfonamide)

Synonyms:N,N′-(6,6′-(2,2-dimethyl-1,3-dioxolane-4,5-diyl)bis-(methylene)bis(oxy)bis(5-(2-methoxy phenoxy)-2,2′-bipyrimidine-6,4-diyl))bis(4-tert-butylbenzenesulfonamide)

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Chemical Property of N,N′-(6,6′-(2,2-dimethyl-1,3-dioxolane-4,5-diyl)bis-(methylene)bis(oxy)bis(5-(2-methoxy phenoxy)-2,2′-bipyrimidine-6,4-diyl))bis(4-tert-butylbenzenesulfonamide)

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Technology Process of N,N′-(6,6′-(2,2-dimethyl-1,3-dioxolane-4,5-diyl)bis-(methylene)bis(oxy)bis(5-(2-methoxy phenoxy)-2,2′-bipyrimidine-6,4-diyl))bis(4-tert-butylbenzenesulfonamide)

There total 3 articles about N,N′-(6,6′-(2,2-dimethyl-1,3-dioxolane-4,5-diyl)bis-(methylene)bis(oxy)bis(5-(2-methoxy phenoxy)-2,2′-bipyrimidine-6,4-diyl))bis(4-tert-butylbenzenesulfonamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 2,2-dimethyl-4,5-di(hydroxymethyl)-1,3-dioxolane

: 150727-06-3
4-tert-butyl-N-(6-chloro-5-(2-methoxyphenoxy)2,2'-bipyrimidin-4-yl)benzene sulfonamide

: 1448588-52-0
N,N′-(6,6′-(2,2-dimethyl-1,3-dioxolane-4,5-diyl)bis-(methylene)bis(oxy)bis(5-(2-methoxy phenoxy)-2,2′-bipyrimidine-6,4-diyl))bis(4-tert-butylbenzenesulfonamide)

Guidance literature:: 2,2-dimethyl-4,5-di(hydroxymethyl)-1,3-dioxolane; With sodium hydroxide; In acetonitrile; at 80 - 85 ℃; for 4h;

4-tert-butyl-N-(6-chloro-5-(2-methoxyphenoxy)2,2'-bipyrimidin-4-yl)benzene sulfonamide; In acetonitrile; at 80 - 85 ℃; for 14h; Solvent; Temperature; Reagent/catalyst;
DOI:10.1021/op400100s

Reference yield:

: 6292-59-7
4-tert-butylbenzenesulphonamide

: 1448588-52-0
N,N′-(6,6′-(2,2-dimethyl-1,3-dioxolane-4,5-diyl)bis-(methylene)bis(oxy)bis(5-(2-methoxy phenoxy)-2,2′-bipyrimidine-6,4-diyl))bis(4-tert-butylbenzenesulfonamide)

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / toluene / 0.5 h / 50 °C / Large scale

1.2: 10 h / 110 °C / Large scale

2.1: sodium hydroxide / acetonitrile / 4 h / 80 - 85 °C

2.2: 14 h / 80 - 85 °C

With potassium carbonate; sodium hydroxide; In toluene; acetonitrile;
DOI:10.1021/op400100s

Reference yield:

: 150728-13-5
4,6-dichloro-5-(2-methoxyphenoxy)-2,2'-bipyrimidine

: 1448588-52-0
N,N′-(6,6′-(2,2-dimethyl-1,3-dioxolane-4,5-diyl)bis-(methylene)bis(oxy)bis(5-(2-methoxy phenoxy)-2,2′-bipyrimidine-6,4-diyl))bis(4-tert-butylbenzenesulfonamide)

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / toluene / 0.5 h / 50 °C / Large scale

1.2: 10 h / 110 °C / Large scale

2.1: sodium hydroxide / acetonitrile / 4 h / 80 - 85 °C

2.2: 14 h / 80 - 85 °C

With potassium carbonate; sodium hydroxide; In toluene; acetonitrile;
DOI:10.1021/op400100s