3-[(1S,2R)-1-(tert-Butyl-dimethyl-silanyloxy)-2-methyl-but-3-enyl]-2,5-dimethoxy-phenylamine

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Chemical Name:3-[(1S,2R)-1-(tert-Butyl-dimethyl-silanyloxy)-2-methyl-but-3-enyl]-2,5-dimethoxy-phenylamine
CAS No.:860613-27-0
Molecular Formula:C₁₉H₃₃NO₃Si
Molecular Weight:351.561
Hs Code.:

Synonyms:3-[(1S,2R)-1-(tert-Butyl-dimethyl-silanyloxy)-2-methyl-but-3-enyl]-2,5-dimethoxy-phenylamine

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Chemical Property of 3-[(1S,2R)-1-(tert-Butyl-dimethyl-silanyloxy)-2-methyl-but-3-enyl]-2,5-dimethoxy-phenylamine

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Technology Process of 3-[(1S,2R)-1-(tert-Butyl-dimethyl-silanyloxy)-2-methyl-but-3-enyl]-2,5-dimethoxy-phenylamine

There total 3 articles about 3-[(1S,2R)-1-(tert-Butyl-dimethyl-silanyloxy)-2-methyl-but-3-enyl]-2,5-dimethoxy-phenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: tert-Butyl-[(1S,2R)-1-(2,5-dimethoxy-3-nitro-phenyl)-2-methyl-but-3-enyloxy]-dimethyl-silane

: 860613-27-0
3-[(1S,2R)-1-(tert-Butyl-dimethyl-silanyloxy)-2-methyl-but-3-enyl]-2,5-dimethoxy-phenylamine

Guidance literature:: With sulfur; sodium tetrahydroborate; In tetrahydrofuran; at 65 ℃;
DOI:10.1002/anie.200500247

Reference yield:

: 860613-34-9
(1S,2R)-1-(2,5-Dimethoxy-3-nitro-phenyl)-2-methyl-but-3-en-1-ol

: 860613-27-0
3-[(1S,2R)-1-(tert-Butyl-dimethyl-silanyloxy)-2-methyl-but-3-enyl]-2,5-dimethoxy-phenylamine

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / -78 °C

2: NaBH₄; S₈ / tetrahydrofuran / 65 °C

With sulfur; sodium tetrahydroborate; triethylamine; In tetrahydrofuran;
DOI:10.1002/anie.200500247

Reference yield:

: 74422-90-5
2,5-dimethoxy-3-nitrobenzaldehyde

: 860613-27-0
3-[(1S,2R)-1-(tert-Butyl-dimethyl-silanyloxy)-2-methyl-but-3-enyl]-2,5-dimethoxy-phenylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / CH₂Cl₂ / -78 - 25 °C

2: Et₃N / -78 °C

3: NaBH₄; S₈ / tetrahydrofuran / 65 °C

With sulfur; sodium tetrahydroborate; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1002/anie.200500247