5'-O-[N-(3-chloro-2-hydroxybenzoyl)sulfamoyl]-2',3'-O-isopropylideneadenosine

Base Information

Chemical Name:5'-O-[N-(3-chloro-2-hydroxybenzoyl)sulfamoyl]-2',3'-O-isopropylideneadenosine
CAS No.:939794-70-4
Molecular Formula:C₂₀H₂₁ClN₆O₈S
Molecular Weight:540.941
Hs Code.:

Synonyms:5'-O-[N-(3-chloro-2-hydroxybenzoyl)sulfamoyl]-2',3'-O-isopropylideneadenosine

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Chemical Property of 5'-O-[N-(3-chloro-2-hydroxybenzoyl)sulfamoyl]-2',3'-O-isopropylideneadenosine

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Technology Process of 5'-O-[N-(3-chloro-2-hydroxybenzoyl)sulfamoyl]-2',3'-O-isopropylideneadenosine

There total 2 articles about 5'-O-[N-(3-chloro-2-hydroxybenzoyl)sulfamoyl]-2',3'-O-isopropylideneadenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: 1829-32-9
3-Chloro-2-hydroxybenzoic acid

: 112921-00-3
((3aR,4R,6R,6aR)-6-(6-amino-9H-purin-9-yl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methyl sulfamate

: 939794-70-4
5'-O-[N-(3-chloro-2-hydroxybenzoyl)sulfamoyl]-2',3'-O-isopropylideneadenosine

Guidance literature:: 3-Chloro-2-hydroxybenzoic acid; With 1,1'-carbonyldiimidazole; In N,N-dimethyl-formamide; at 60 ℃; for 2h;

((3aR,4R,6R,6aR)-6-(6-amino-9H-purin-9-yl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methyl sulfamate; In N,N-dimethyl-formamide; at 20 ℃; for 3h; Further stages.;
DOI:10.1021/jm070905o