methyl 5-(N-(4-cyclohexylbenzyl)-2-(N,4-dimethylphenylsulfonamido)acetamido)-2-hydroxybenzoate

Base Information

Chemical Name:methyl 5-(N-(4-cyclohexylbenzyl)-2-(N,4-dimethylphenylsulfonamido)acetamido)-2-hydroxybenzoate
CAS No.:1456601-83-4
Molecular Formula:C₃₁H₃₆N₂O₆S
Molecular Weight:564.703
Hs Code.:

Synonyms:methyl 5-(N-(4-cyclohexylbenzyl)-2-(N,4-dimethylphenylsulfonamido)acetamido)-2-hydroxybenzoate

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Chemical Property of methyl 5-(N-(4-cyclohexylbenzyl)-2-(N,4-dimethylphenylsulfonamido)acetamido)-2-hydroxybenzoate

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Technology Process of methyl 5-(N-(4-cyclohexylbenzyl)-2-(N,4-dimethylphenylsulfonamido)acetamido)-2-hydroxybenzoate

There total 6 articles about methyl 5-(N-(4-cyclohexylbenzyl)-2-(N,4-dimethylphenylsulfonamido)acetamido)-2-hydroxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 2644-99-7
2-(N-methyl-N-(p-toluenesulfonamido))acetic acid

: 1456601-57-2
methyl 5-(4-cyclohexylbenzylamino)-2-hydroxybenzoate

: 1456601-83-4
methyl 5-(N-(4-cyclohexylbenzyl)-2-(N,4-dimethylphenylsulfonamido)acetamido)-2-hydroxybenzoate

Guidance literature:: With dichlorotriphenylphosphorane; In dichloromethane; at 80 ℃; for 1h; Inert atmosphere; Microwave irradiation;
DOI:10.1039/c3md20323a

Reference yield:

: 42753-75-3
methyl 5-amino-2-hydroxybenzoate

: 1456601-83-4
methyl 5-(N-(4-cyclohexylbenzyl)-2-(N,4-dimethylphenylsulfonamido)acetamido)-2-hydroxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic acid / methanol / 1 h / 20 - 40 °C / Molecular sieve

1.2: 2 h / 5 - 20 °C

2.1: dichlorotriphenylphosphorane / dichloromethane / 1 h / 80 °C / Inert atmosphere; Microwave irradiation

With acetic acid; dichlorotriphenylphosphorane; In methanol; dichloromethane;
DOI:10.1039/c3md20323a

Reference yield:

: 28126-01-4
methyl 2-(N,4-dimethylphenylsulfonam ido)acetate

: 1456601-83-4
methyl 5-(N-(4-cyclohexylbenzyl)-2-(N,4-dimethylphenylsulfonamido)acetamido)-2-hydroxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: lithium hydroxide / methanol; tetrahydrofuran; water / 20 °C

2: dichlorotriphenylphosphorane / dichloromethane / 1 h / 80 °C / Inert atmosphere; Microwave irradiation

With lithium hydroxide; dichlorotriphenylphosphorane; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1039/c3md20323a