1-<4-<2-(diethylamino)ethoxy>phenyl>-1-phenyl-2-chloro-2-<3-methoxy-4-(benzyloxy)phenyl>ethene

Base Information

Chemical Name:1-<4-<2-(diethylamino)ethoxy>phenyl>-1-phenyl-2-chloro-2-<3-methoxy-4-(benzyloxy)phenyl>ethene
CAS No.:117095-61-1
Molecular Formula:C₃₄H₃₆ClNO₃
Molecular Weight:542.118
Hs Code.:

Synonyms:1-<4-<2-(diethylamino)ethoxy>phenyl>-1-phenyl-2-chloro-2-<3-methoxy-4-(benzyloxy)phenyl>ethene

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Chemical Property of 1-<4-<2-(diethylamino)ethoxy>phenyl>-1-phenyl-2-chloro-2-<3-methoxy-4-(benzyloxy)phenyl>ethene

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Technology Process of 1-<4-<2-(diethylamino)ethoxy>phenyl>-1-phenyl-2-chloro-2-<3-methoxy-4-(benzyloxy)phenyl>ethene

There total 4 articles about 1-<4-<2-(diethylamino)ethoxy>phenyl>-1-phenyl-2-chloro-2-<3-methoxy-4-(benzyloxy)phenyl>ethene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 117095-63-3
1-<4-<2-(diethylamino)ethoxy>phenyl>-1-phenyl-2-hydroxy-2-<3-methoxy-4-(benzyloxy)phenyl>ethene

: 117095-61-1
1-<4-<2-(diethylamino)ethoxy>phenyl>-1-phenyl-2-chloro-2-<3-methoxy-4-(benzyloxy)phenyl>ethene

Guidance literature:: With N-chloro-succinimide; In chloroform; for 3h; Heating;
DOI:10.1021/jm00121a035

Reference yield:

: 2426-87-1
3-methoxy-4-(phenylmethoxy)benzaldehyde

: 117095-61-1
1-<4-<2-(diethylamino)ethoxy>phenyl>-1-phenyl-2-chloro-2-<3-methoxy-4-(benzyloxy)phenyl>ethene

Guidance literature:: Multi-step reaction with 2 steps

1: 36 percent / 1) TiCl₄, Zn / tetrahydrofuran / 1) reflux, 2 h, 2) r.t.

2: 75 percent / N-chlorosuccinimide / CHCl₃ / 3 h / Heating

With N-chloro-succinimide; titanium tetrachloride; zinc; In tetrahydrofuran; chloroform;
DOI:10.1021/jm00121a035

Reference yield:

: 100-44-7
benzyl chloride

: 117095-61-1
1-<4-<2-(diethylamino)ethoxy>phenyl>-1-phenyl-2-chloro-2-<3-methoxy-4-(benzyloxy)phenyl>ethene

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / 1) NaH / 1) DMF, 2) 125 deg C, 4 h

2: 36 percent / 1) TiCl₄, Zn / tetrahydrofuran / 1) reflux, 2 h, 2) r.t.

3: 75 percent / N-chlorosuccinimide / CHCl₃ / 3 h / Heating

With N-chloro-succinimide; titanium tetrachloride; sodium hydride; zinc; In tetrahydrofuran; chloroform;
DOI:10.1021/jm00121a035