C₉H₇O₃^(1-)*Na⁽¹⁺⁾

Base Information

• Chemical Name: C₉H₇O₃^(1-)*Na⁽¹⁺⁾
• CAS No.: 1403763-90-5
• Molecular Formula: C₉H₇O₃*Na
• Molecular Weight: 186.143
• Mol file: 1403763-90-5.mol

Synonyms:C₉H₇O₃^(1-)*Na⁽¹⁺⁾

Chemical Property of C₉H₇O₃^(1-)*Na⁽¹⁺⁾

Chemical Property:

Purity/Quality:

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Technology Process of C₉H₇O₃^(1-)*Na⁽¹⁺⁾

There total 1 articles about C₉H₇O₃^(1-)*Na⁽¹⁺⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

o-hydroxyacetophenone (118-93-4,104809-67-8) + formic acid ethyl ester (109-94-4) → C9H7O3(1-)*Na(1+) (1403763-90-5)

Guidance literature:

With sodium; for 2h; Reflux; Inert atmosphere; neat (no solvent);

DOI:10.1055/s-0031-1289789

Reference yield:

C9H7O3(1-)*Na(1+) (1403763-90-5) → 3(5)-(2'-hydroxyphenyl)pyrazole (34810-67-8)

Guidance literature:

With hydrazine hydrate; acetic acid; In ethanol; for 5h; Reflux; Inert atmosphere;

DOI:10.1016/j.tet.2013.12.026

upstream raw materials:

o-hydroxyacetophenone

formic acid ethyl ester

Downstream raw materials:

3⁽⁵⁾-(2'-hydroxyphenyl)pyrazole