5-[2-chloro-4-(3,5-dioxo-4,5-dihydro-3H-[1,2,4]triazin-2-yl)-6-methyl-phenoxy]-2-methoxy-benzaldehyde

Base Information

• Chemical Name: 5-[2-chloro-4-(3,5-dioxo-4,5-dihydro-3H-[1,2,4]triazin-2-yl)-6-methyl-phenoxy]-2-methoxy-benzaldehyde
• CAS No.: 660408-07-1
• Molecular Formula: C₁₈H₁₄ClN₃O₅
• Molecular Weight: 387.779

Synonyms:5-[2-chloro-4-(3,5-dioxo-4,5-dihydro-3H-[1,2,4]triazin-2-yl)-6-methyl-phenoxy]-2-methoxy-benzaldehyde

Chemical Property of 5-[2-chloro-4-(3,5-dioxo-4,5-dihydro-3H-[1,2,4]triazin-2-yl)-6-methyl-phenoxy]-2-methoxy-benzaldehyde

Chemical Property:

Purity/Quality:

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Technology Process of 5-[2-chloro-4-(3,5-dioxo-4,5-dihydro-3H-[1,2,4]triazin-2-yl)-6-methyl-phenoxy]-2-methoxy-benzaldehyde

There total 1 articles about 5-[2-chloro-4-(3,5-dioxo-4,5-dihydro-3H-[1,2,4]triazin-2-yl)-6-methyl-phenoxy]-2-methoxy-benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

hexamethylenetetramine (100-97-0) + 2-{3-chloro-4-[4-methoxy-phenoxy]-5-methyl-phenyl}-2H-[1,2,4]triazine-3,5-dione → 5-[2-chloro-4-(3,5-dioxo-4,5-dihydro-3H-[1,2,4]triazin-2-yl)-6-methyl-phenoxy]-2-methoxy-benzaldehyde (660408-07-1)

Guidance literature:

With trifluoroacetic acid; Heating;

DOI:10.1016/S0960-894X(02)00947-2

Reference yield: 79.0%

5-[2-chloro-4-(3,5-dioxo-4,5-dihydro-3H-[1,2,4]triazin-2-yl)-6-methyl-phenoxy]-2-methoxy-benzaldehyde (660408-07-1) → 5-[2-chloro-4-(3,5-dioxo-4,5-dihydro-3H-[1,2,4]triazin-2-yl)-6-methyl-phenoxy]-2-methoxy-benzoic acid (660408-11-7)

Guidance literature:

With sodium chlorite; potassium dihydrogenphosphate; 2-Methyl-1-butene; In tetrahydrofuran; tert-butyl alcohol;

DOI:10.1016/S0960-894X(02)00947-2

Reference yield:

5-[2-chloro-4-(3,5-dioxo-4,5-dihydro-3H-[1,2,4]triazin-2-yl)-6-methyl-phenoxy]-2-methoxy-benzaldehyde (660408-07-1) → 5-[2-chloro-4-(3,5-dioxo-4,5-dihydro-3H-[1,2,4]triazin-2-yl)-6-methyl-phenoxy]-2-hydroxy-benzoic acid (660409-78-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 79 percent / aq. NaClO₂; KH₂PO₄; 2-methylbutene / 2-methyl-propan-2-ol; tetrahydrofuran

2: 78 percent / BCl₃ / CH₂Cl₂ / -78 - 20 °C

With sodium chlorite; potassium dihydrogenphosphate; boron trichloride; 2-Methyl-1-butene; In tetrahydrofuran; dichloromethane; tert-butyl alcohol;

DOI:10.1016/S0960-894X(02)00947-2

upstream raw materials:

hexamethylenetetramine

Downstream raw materials:

5-[2-chloro-4-(3,5-dioxo-4,5-dihydro-3H-[1,2,4]triazin-2-yl)-6-methyl-phenoxy]-2-methoxy-benzoic acid

5-[2-chloro-4-(3,5-dioxo-4,5-dihydro-3H-[1,2,4]triazin-2-yl)-6-methyl-phenoxy]-2-hydroxy-benzoic acid

5-[2-chloro-4-(3,5-dioxo-4,5-dihydro-3H-[1,2,4]triazin-2-yl)-6-methyl-phenoxy]-2-hydroxy-benzoic acid 2,5-dioxo-pyrrolidin-1-yl ester

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