25,27-bis(N-{1-[4-({3-[4-(tert-butyl)phenyl]-5-isoxazolyl}methoxy)phenyl]aminocarbonyl}methoxy)-26,28-dihydroxycalix[4]arene

Base Information

Chemical Name:25,27-bis(N-{1-[4-({3-[4-(tert-butyl)phenyl]-5-isoxazolyl}methoxy)phenyl]aminocarbonyl}methoxy)-26,28-dihydroxycalix[4]arene
CAS No.:1291082-83-1
Molecular Formula:C₇₂H₆₈N₄O₁₀
Molecular Weight:1149.35
Hs Code.:

Synonyms:25,27-bis(N-{1-[4-({3-[4-(tert-butyl)phenyl]-5-isoxazolyl}methoxy)phenyl]aminocarbonyl}methoxy)-26,28-dihydroxycalix[4]arene

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Chemical Property of 25,27-bis(N-{1-[4-({3-[4-(tert-butyl)phenyl]-5-isoxazolyl}methoxy)phenyl]aminocarbonyl}methoxy)-26,28-dihydroxycalix[4]arene

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Technology Process of 25,27-bis(N-{1-[4-({3-[4-(tert-butyl)phenyl]-5-isoxazolyl}methoxy)phenyl]aminocarbonyl}methoxy)-26,28-dihydroxycalix[4]arene

There total 5 articles about 25,27-bis(N-{1-[4-({3-[4-(tert-butyl)phenyl]-5-isoxazolyl}methoxy)phenyl]aminocarbonyl}methoxy)-26,28-dihydroxycalix[4]arene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1291079-72-5
4-[3-(4-tert-butyl-phenyl)-isoxazol-5-ylmethoxy]-phenylamine

: 337515-06-7
C₃₂H₂₆Cl₂O₆

: 1291082-83-1
25,27-bis(N-{1-[4-({3-[4-(tert-butyl)phenyl]-5-isoxazolyl}methoxy)phenyl]aminocarbonyl}methoxy)-26,28-dihydroxycalix[4]arene

Guidance literature:: With triethylamine; In dichloromethane; at 40 ℃; for 24h; Inert atmosphere;
DOI:10.1002/ejoc.201001169

Reference yield:

: 1291079-77-0
3-(4-tert-butyl-phenyl)-5-(4-nitro-phenoxymethyl)-isoxazole

: 1291082-83-1
25,27-bis(N-{1-[4-({3-[4-(tert-butyl)phenyl]-5-isoxazolyl}methoxy)phenyl]aminocarbonyl}methoxy)-26,28-dihydroxycalix[4]arene

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium formate; zinc / methanol / 20 °C

2: triethylamine / dichloromethane / 24 h / 40 °C / Inert atmosphere

With ammonium formate; triethylamine; zinc; In methanol; dichloromethane;
DOI:10.1002/ejoc.201001169

Reference yield:

: 189164-19-0
25,27-bis(methoxycarboxylic acid)-26,28-dihydroxycalix[4]arene

: 1291082-83-1
25,27-bis(N-{1-[4-({3-[4-(tert-butyl)phenyl]-5-isoxazolyl}methoxy)phenyl]aminocarbonyl}methoxy)-26,28-dihydroxycalix[4]arene

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 20 °C / Inert atmosphere; Reflux

2: triethylamine / dichloromethane / 24 h / 40 °C / Inert atmosphere

With oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1002/ejoc.201001169