(+/-)-2-(2-chlorophenyl)-N'-(3,5-dichlorophenyl)-2-(4-methyl-1-piperazinyl)acetohydrazide

Base Information

Chemical Name:(+/-)-2-(2-chlorophenyl)-N'-(3,5-dichlorophenyl)-2-(4-methyl-1-piperazinyl)acetohydrazide
CAS No.:1092476-46-4
Molecular Formula:C₁₉H₂₁Cl₃N₄O
Molecular Weight:427.761
Hs Code.:

Synonyms:(+/-)-2-(2-chlorophenyl)-N'-(3,5-dichlorophenyl)-2-(4-methyl-1-piperazinyl)acetohydrazide

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Chemical Property of (+/-)-2-(2-chlorophenyl)-N'-(3,5-dichlorophenyl)-2-(4-methyl-1-piperazinyl)acetohydrazide

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Technology Process of (+/-)-2-(2-chlorophenyl)-N'-(3,5-dichlorophenyl)-2-(4-methyl-1-piperazinyl)acetohydrazide

There total 3 articles about (+/-)-2-(2-chlorophenyl)-N'-(3,5-dichlorophenyl)-2-(4-methyl-1-piperazinyl)acetohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1092477-37-6
(+/-)-(2-chlorophenyl)(4-methyl-1-piperazinyl)acetic acid hydrochloride

: 39943-56-1
3,5-dichlorophenylhydrazine

: 1092476-46-4
(+/-)-2-(2-chlorophenyl)-N'-(3,5-dichlorophenyl)-2-(4-methyl-1-piperazinyl)acetohydrazide

Guidance literature:: (+/-)-(2-chlorophenyl)(4-methyl-1-piperazinyl)acetic acid hydrochloride; With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; In dichloromethane; at 20 ℃; for 0.166667h;

3,5-dichlorophenylhydrazine; In dichloromethane; at 20 ℃; for 4h;

Reference yield:

: 29270-30-2,141109-25-3
α-bromo-2-chlorophenyl acetic acid

: 1092476-46-4
(+/-)-2-(2-chlorophenyl)-N'-(3,5-dichlorophenyl)-2-(4-methyl-1-piperazinyl)acetohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / tetrahydrofuran / 20 °C

2.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / dichloromethane / 0.17 h / 20 °C

2.2: 4 h / 20 °C

With potassium carbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; In tetrahydrofuran; dichloromethane;

Reference yield:

: 2444-36-2
2'-chloro-benzeneacetic acid

: 1092476-46-4
(+/-)-2-(2-chlorophenyl)-N'-(3,5-dichlorophenyl)-2-(4-methyl-1-piperazinyl)acetohydrazide

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 5 h / 80 °C

2.1: potassium carbonate / tetrahydrofuran / 20 °C

3.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / dichloromethane / 0.17 h / 20 °C

3.2: 4 h / 20 °C

With N-Bromosuccinimide; potassium carbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; dibenzoyl peroxide; In tetrahydrofuran; tetrachloromethane; dichloromethane;