12-(4-Dimethylamino-phenyl)-9,9-dimethyl-9,10-dihydro-8H-benzo[a]acridin-11-one

Base Information

• Chemical Name: 12-(4-Dimethylamino-phenyl)-9,9-dimethyl-9,10-dihydro-8H-benzo[a]acridin-11-one
• CAS No.: 128225-16-1
• Molecular Formula: C₂₇H₂₆N₂O
• Molecular Weight: 394.516
• Mol file: 128225-16-1.mol

Synonyms:12-(4-Dimethylamino-phenyl)-9,9-dimethyl-9,10-dihydro-8H-benzo[a]acridin-11-one

Chemical Property of 12-(4-Dimethylamino-phenyl)-9,9-dimethyl-9,10-dihydro-8H-benzo[a]acridin-11-one

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 12-(4-Dimethylamino-phenyl)-9,9-dimethyl-9,10-dihydro-8H-benzo[a]acridin-11-one

There total 4 articles about 12-(4-Dimethylamino-phenyl)-9,9-dimethyl-9,10-dihydro-8H-benzo[a]acridin-11-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

12-(4-dimethylaminophenyl)-9,9-dimethyl-8,9,10,12-tetrahydro-7H-benzo[a]acridin-11-one (128225-09-2) → 12-(4-Dimethylamino-phenyl)-9,9-dimethyl-9,10-dihydro-8H-benzo[a]acridin-11-one (128225-16-1)

Guidance literature:

With chromium(VI) oxide; In acetic acid;

Reference yield:

dimedone (3471-13-4) → 12-(4-Dimethylamino-phenyl)-9,9-dimethyl-9,10-dihydro-8H-benzo[a]acridin-11-one (128225-16-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 35 percent / ethanol / Heating

2: 95 percent / CrO₃ / acetic acid

With chromium(VI) oxide; In ethanol; acetic acid;

Reference yield:

4-dimethylamino-benzaldehyde (100-10-7) → 12-(4-Dimethylamino-phenyl)-9,9-dimethyl-9,10-dihydro-8H-benzo[a]acridin-11-one (128225-16-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 35 percent / ethanol / Heating

2: 95 percent / CrO₃ / acetic acid

With chromium(VI) oxide; In ethanol; acetic acid;

upstream raw materials:

12-(4-dimethylaminophenyl)-9,9-dimethyl-8,9,10,12-tetrahydro-7H-benzo[a]acridin-11-one

dimedone

naphthalen-2-ylamine

4-dimethylamino-benzaldehyde